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[ CAS No. 1417713-93-9 ] {[proInfo.proName]}

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Chemical Structure| 1417713-93-9
Chemical Structure| 1417713-93-9
Structure of 1417713-93-9 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1417713-93-9 ]

CAS No. :1417713-93-9 MDL No. :
Formula : C33H30O9 Boiling Point : -
Linear Structure Formula :- InChI Key :OXBIDZVLELTOEU-UHFFFAOYSA-N
M.W : 570.59 Pubchem ID :91810419
Synonyms :

Safety of [ 1417713-93-9 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 1417713-93-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1417713-93-9 ]

[ 1417713-93-9 ] Synthesis Path-Downstream   1~5

  • 1
  • copper(II) nitrate trihydrate [ No CAS ]
  • [ 127-19-5 ]
  • [ 1417713-93-9 ]
  • 4C33H27O9(3-)*12Cu(2+)*30H2O*37C4H9NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
53% at 85℃; for 72h;
  • 2
  • cadmium(II) nitrate tetrhydrate [ No CAS ]
  • [ 1417713-93-9 ]
  • [ 7732-18-5 ]
  • [ 33513-42-7 ]
  • 17Cd(2+)*12C33H27O9(3-)*2C3H7NO*6H2O*2C2H8N(1+) [ No CAS ]
YieldReaction ConditionsOperation in experiment
at 95℃; for 72h; Sealed tube;
  • 3
  • [ 21988-87-4 ]
  • [ 19438-10-9 ]
  • [ 1417713-93-9 ]
YieldReaction ConditionsOperation in experiment
Stage #1: 1,3,5-tris(bromomethyl)-2,4,6-trimethylbenzene; methyl 3-hydroxybenzoate With potassium carbonate In N,N-dimethyl-formamide at 90℃; for 96h; Stage #2: With water; potassium hydroxide In tetrahydrofuran; ethanol at 90℃; for 6h; Synthesis of ligand TTBA 5 mmol of compound 1, 15 mmol of compound 2 and45 mmol of K2CO3 were dissolved in 250 ml DMF and then heated to 90 °C andstirred at this temperature for 96 h. After cooling to room temperature, a lot ofwater was added into the above mixture and afforded a large number of precipitates.The precipitate was dissolved in the mixed solvents of 50 ml H2O, 80 mlEtOH and 60 ml THF containing 4.5 g KOH, then the mixture was hydrolyzed at90 °C for 6 h. The solvent was removed and water was added and the pH wastuned to about 3. The white precipitate was obtained and filtered and dried at 60 °C. 1H NMR (DMSO-d6): δ 2.40 (s, 9H), 5.18 (s, 6H), 7.31 (d, 3H), 7.45 (t, 3H),7.56-7.60 (m, 6H), 13.0 (s, 3H)
  • 4
  • [ 872-50-4 ]
  • terbium(III) nitrate hexahydrate [ No CAS ]
  • [ 1417713-93-9 ]
  • [ 33513-42-7 ]
  • [terbium(III)(2,4,6-tris[1-(3-carboxylatophenoxy)ylmethyl]mesitylene)(H2O)](H2O)4(N,N-dimethylformamide)(N-methyl-2-pyrrolidone)0.5 [ No CAS ]
YieldReaction ConditionsOperation in experiment
62% In formic acid at 140℃; for 72h; Sealed tube; Autoclave;
  • 5
  • [ 1417713-93-9 ]
  • [ 1079-66-9 ]
  • [ 116911-32-1 ]
  • C99H90N3O15P3 [ No CAS ]
YieldReaction ConditionsOperation in experiment
63% Stage #1: 3,3',3”-(((2,4,6-trimethylbenzene-1,3,5-triyl)tris(methylene))tris(oxy))tribenzoic acid; chloro-diphenylphosphine With triethylamine In toluene at 20℃; for 0.166667h; Stage #2: (S)-2-azido-3-phenylpropionic acid methyl ester In toluene at 25℃; for 8h; 31 Example 31 In the reactor, add 0.2 mmol3,3',3”-(((2,4,6-trimethylbenzene-1,3,5-triyl)tris(methylene))tris(oxy))tribenzoic acid and 1 ml Toluene,Then add 0.6 millimoles of chlorodiphenyl phosphine and 0.72 millimoles of triethylamine, and stir at room temperature for 10 minutes,Add 0.6 millimoles of azide derived from L-phenylalanine methyl ester and react at 25°C for 8 hours,The reaction solution directly used the eluent (V petroleum ether:V ethyl acetate=1:4) to obtain N-acyl phosphoramide compound 6aai through silica gel column chromatography, with a yield of 63%, a colorless oily liquid.
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