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Chemical Structure| 1421601-23-1 Chemical Structure| 1421601-23-1

Structure of 1421601-23-1

Chemical Structure| 1421601-23-1

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Product Details of [ 1421601-23-1 ]

CAS No. :1421601-23-1
Formula : C5H10ClNO2
M.W : 151.59
SMILES Code : O=C(C1(CN)CC1)O.[H]Cl
MDL No. :MFCD13469300
InChI Key :SRTXENKRXZLJHQ-UHFFFAOYSA-N
Pubchem ID :53433553

Safety of [ 1421601-23-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 1421601-23-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1421601-23-1 ]

[ 1421601-23-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 6914-79-0 ]
  • [ 1421601-23-1 ]
YieldReaction ConditionsOperation in experiment
97% With hydrogenchloride; platinum(IV) oxide; hydrogen; In methanol; at 20℃; for 4h; Preparational Example 1 Preparation of 1-(aminomethyl)-cyclopropylacetic acid hydrochloride 200 mg (1.75 mmol) of 1-cyano-1-cyclopropylacetic acid was dissolved in 10 ml of methanol, to which 40 mg (20 wt percent) of platinum oxide was added. 0.3 ml of concentrated hydrochloric acid solution was loaded thereto, and the mixture was stirred at room temperature for 4 hours in hydrogen stream. Upon completion of the reaction, the mixture was filtered to eliminate platinum oxide. The solvent was evaporated under reduced pressure to give 256 mg of 1-(aminomethyl)-cyclopropylacetic acid hydrochloride (yield: 97percent). 1H NMR (400 MHz, MeOD) delta 3.13 (s, 2H), 1.36-1.38 (m, 2H), 1.16-1.18 (m, 2H)
 

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[ 1421601-23-1 ]

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