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[ CAS No. 1429436-06-5 ] {[proInfo.proName]}

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Chemical Structure| 1429436-06-5
Chemical Structure| 1429436-06-5
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Product Details of [ 1429436-06-5 ]

CAS No. :1429436-06-5 MDL No. :N/A
Formula : C19H13NO4 Boiling Point : -
Linear Structure Formula :- InChI Key :DMZIXVHACOAZQC-UHFFFAOYSA-N
M.W : 319.31 Pubchem ID :102206428
Synonyms :

Safety of [ 1429436-06-5 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 1429436-06-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1429436-06-5 ]

[ 1429436-06-5 ] Synthesis Path-Downstream   1~29

  • 1
  • [ 625-92-3 ]
  • [ 25487-66-5 ]
  • [ 1429436-06-5 ]
  • 2
  • [ 1429436-06-5 ]
  • C19H11Cl2NO2 [ No CAS ]
  • 3
  • [ 1429436-06-5 ]
  • [ 1429436-03-2 ]
  • 4
  • zinc(II) nitrate hexahydrate [ No CAS ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [ 1521181-78-1 ]
YieldReaction ConditionsOperation in experiment
75% With 4-nitro-benzoic acid; In N,N-dimethyl acetamide; at 160℃; for 72h; A mixture of H2pddb (0.0128g, 0.04mmol), Zn(NO3)2·6H2O (0.0297g, 0.1mmol), 4-nitrobenzoic acid (0.0146g, 0.10mmol), water (6mL), and DMA (1mL) was heated in 25mL Teflon-lined stainless steel container at 160C for three days, and slowly cooled to room temperature at a rate of 5C/h. Then colorless block crystals 1 were obtained with a 75% yield (based on H2pddb) after being washed several times by water. Elemental analysis: Anal. Calc. for C19H13NO5Zn: C, 56.95; H, 3.17; N, 3.50. Found: C, 56.79; H, 3.34; N, 3.33%. IR (KBr, cm-1): 3421 (bw), 3053 (bw), 1612 (w), 1542 (s), 1397 (s), 1277 (w), 1172 (w), 820 (w), 766 (m), 690 (m).
  • 5
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • cadmium(II) iodide [ No CAS ]
  • [Cd2(pddb)2]·H2O}n [ No CAS ]
YieldReaction ConditionsOperation in experiment
70% With N,N-dimethyl acetamide; 4-nitro-benzoic acid; In N,N-dimethyl acetamide; acetonitrile; at 160℃; for 72h; A mixture of H2pddb (0.0128g, 0.04mmol), CdI2 (0.0366g, 0.1mmol), 4-nitrobenzoic acid (0.0146g, 0.10mmol), water (6mL), and MeCN (2mL) was heated in 25mL Teflon-lined stainless steel container at 160C for three days, and slowly cooled to room temperature at a rate of 5C/h. Thus, colorless block crystals 3 were achieved with a pure yield of 70% (based on H2pddb). Elemental analysis: Anal. Calc. for C38H24N2O9Cd2: C, 52.12; H, 2.76; N, 3.19. Found: C, 52.21; H, 2.93; N, 3.02%. IR (KBr, cm-1): 3433 (bw), 3081 (w), 2928 (w), 2484 (w), 2249 (w), 1704 (w), 1604 (m), 1557 (s), 1455 (m), 1395 (s), 1349 (s), 1260 (w), 926 (w), 764 (m), 684 (m).
  • 6
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • cadmium(II) iodide [ No CAS ]
  • [Cd(pddb)(H2O)2]n [ No CAS ]
YieldReaction ConditionsOperation in experiment
58% With N,N-dimethyl acetamide; In N,N-dimethyl acetamide; acetonitrile; at 160℃; for 72h; A mixture of H2pddb (0.0128g, 0.04mmol), CdI2 (0.0366g, 0.1mmol), water (6mL), and MeCN (2mL) was heated in 25mL Teflon-lined stainless steel container at 160C for three days, and slowly cooled to room temperature at a rate of 5C/h. Colorless block crystal 4 were collected, and then filtered to get a yield of 58% (based on H2pddb). Elemental analysis: Anal. Calc. for C19H15NO6Cd: C, 49.00; H, 3.25; N, 3.01. Found: C, 48.82; H, 3.40; N, 3.08%. IR (KBr, cm-1): 3391 (bw), 3080 (w), 2926 (w), 1696 (w), 1605 (m), 1557 (s), 1435 (m), 1351 (s), 1253 (w), 1174 (w), 892 (bw), 765 (m), 688 (m), 567 (w).
  • 7
  • zinc(II) nitrate hexahydrate [ No CAS ]
  • [ 1429436-06-5 ]
  • [Zn(pddb)]n [ No CAS ]
YieldReaction ConditionsOperation in experiment
60% With N,N-dimethyl acetamide; In N,N-dimethyl acetamide; water; at 160℃; for 72h; A mixture of H2pddb (0.0128g, 0.04mmol), Zn(NO3)2·6H2O (0.0297g, 0.1mmol), water (6mL), and DMA (1mL) was heated in 25mL Teflon-lined stainless steel container at 160C for three days, and slowly cooled to room temperature at a rate of 5C/h. Meanwhile, colorless stick crystals were collected, with yield of 60% (based on H2pddb). Elemental analysis: Anal. Calc. for C19H11NO4Zn: C, 59.63; H, 2.90; N, 3.66. Found: C, 59.74; H, 2.82; N, 3.76%. IR (KBr, cm-1): 3049 (w), 2360 (w), 1608 (w), 1540 (s), 1395 (s), 820 (w), 764 (m), 682 (m).
  • 8
  • gadolinium(III) nitrate hexahydrate [ No CAS ]
  • [ 127-19-5 ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [Gd3(pyridine-3,5-bis(phenyl-3-carboxylic acid))4(OH)(H2O)2]·DMAC}n [ No CAS ]
  • 9
  • europium(III) nitrate pentahydrate [ No CAS ]
  • [ 127-19-5 ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [Eu3(pyridine-3,5-bis(phenyl-3-carboxylic acid))4(OH)(H2O)2]·DMAC}n [ No CAS ]
  • 10
  • terbium(III) nitrate hexahydrate [ No CAS ]
  • gadolinium(III) nitrate hexahydrate [ No CAS ]
  • europium(III) nitrate pentahydrate [ No CAS ]
  • [ 127-19-5 ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [(Gd0.81Tb0.1Eu0.09)3(pyridine-3,5-bis(phenyl-3-carboxylic acid))4(OH)(H2O)2]·DMAC} [ No CAS ]
  • 11
  • terbium(III) nitrate hexahydrate [ No CAS ]
  • gadolinium(III) nitrate hexahydrate [ No CAS ]
  • europium(III) nitrate pentahydrate [ No CAS ]
  • [ 127-19-5 ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [(Gd0.75Tb0.18Eu0.07)3(pyridine-3,5-bis(phenyl-3-carboxylic acid))4(OH)(H2O)2]·DMAC} [ No CAS ]
  • 12
  • terbium(III) nitrate hexahydrate [ No CAS ]
  • [ 127-19-5 ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [Tb3(pyridine-3,5-bis(phenyl-3-carboxylic acid))4(OH)(H2O)2]·DMAC}n [ No CAS ]
  • 13
  • [ 617-84-5 ]
  • terbium(III) nitrate hexahydrate [ No CAS ]
  • europium(III) nitrate hexahydrate [ No CAS ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [Tb2.997Eu0.003(3,5-bis(3-carboxyphenyl)pyridine)4(μ-HCOO)(μ-H2O)(H2O)2(N,N-diethylformamide)]n [ No CAS ]
  • 14
  • [ 617-84-5 ]
  • terbium(III) nitrate hexahydrate [ No CAS ]
  • europium(III) nitrate hexahydrate [ No CAS ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [Tb2.994Eu0.006(3,5-bis(3-carboxyphenyl)pyridine)4(μ-HCOO)(μ-H2O)(H2O)2(N,N-diethylformamide)]n [ No CAS ]
  • 15
  • [ 617-84-5 ]
  • terbium(III) nitrate hexahydrate [ No CAS ]
  • europium(III) nitrate hexahydrate [ No CAS ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [Tb2.991Eu0.009(3,5-bis(3-carboxyphenyl)pyridine)4(μ-HCOO)(μ-H2O)(H2O)2(N,N-diethylformamide)]n [ No CAS ]
  • 16
  • [ 617-84-5 ]
  • terbium(III) nitrate hexahydrate [ No CAS ]
  • europium(III) nitrate hexahydrate [ No CAS ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [Tb2.97Eu0.03(3,5-bis(3-carboxyphenyl)pyridine)4(μ-HCOO)(μ-H2O)(H2O)2(N,N-diethylformamide)]n [ No CAS ]
  • 17
  • [ 617-84-5 ]
  • terbium(III) nitrate hexahydrate [ No CAS ]
  • europium(III) nitrate hexahydrate [ No CAS ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [Tb2.94Eu0.06(3,5-bis(3-carboxyphenyl)pyridine)4(μ-HCOO)(μ-H2O)(H2O)2(N,N-diethylformamide)]n [ No CAS ]
  • 18
  • [ 617-84-5 ]
  • terbium(III) nitrate hexahydrate [ No CAS ]
  • europium(III) nitrate hexahydrate [ No CAS ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [Tb2.91Eu0.09(3,5-bis(3-carboxyphenyl)pyridine)4(μ-HCOO)(μ-H2O)(H2O)2(N,N-diethylformamide)]n [ No CAS ]
  • 19
  • [ 617-84-5 ]
  • terbium(III) nitrate hexahydrate [ No CAS ]
  • europium(III) nitrate hexahydrate [ No CAS ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [Tb2.88Eu0.12(3,5-bis(3-carboxyphenyl)pyridine)4(μ-HCOO)(μ-H2O)(H2O)2(N,N-diethylformamide)]n [ No CAS ]
  • 20
  • [ 617-84-5 ]
  • terbium(III) nitrate hexahydrate [ No CAS ]
  • europium(III) nitrate hexahydrate [ No CAS ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [Tb2.7Eu0.3(3,5-bis(3-carboxyphenyl)pyridine)4(μ-HCOO)(μ-H2O)(H2O)2(N,N-diethylformamide)]n [ No CAS ]
  • 21
  • [ 617-84-5 ]
  • terbium(III) nitrate hexahydrate [ No CAS ]
  • europium(III) nitrate hexahydrate [ No CAS ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [Tb2.55Eu0.45(3,5-bis(3-carboxyphenyl)pyridine)4(μ-HCOO)(μ-H2O)(H2O)2(N,N-diethylformamide)]n [ No CAS ]
  • 22
  • [ 617-84-5 ]
  • terbium(III) nitrate hexahydrate [ No CAS ]
  • europium(III) nitrate hexahydrate [ No CAS ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [Tb2.4Eu0.6(3,5-bis(3-carboxyphenyl)pyridine)4(μ-HCOO)(μ-H2O)(H2O)2(N,N-diethylformamide)]n [ No CAS ]
  • 23
  • [ 617-84-5 ]
  • europium(III) nitrate hexahydrate [ No CAS ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [Eu3(3,5-bis(3-carboxyphenyl)pyridine)4(μ-HCOO)(μ-H2O)(H2O)2(N,N-diethylformamide)]n [ No CAS ]
  • 24
  • [ 617-84-5 ]
  • terbium(III) nitrate hexahydrate [ No CAS ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [Tb3(3,5-bis(3-carboxyphenyl)pyridine)4(μ-HCOO)(μ-H2O)(H2O)2(N,N-diethylformamide)]n [ No CAS ]
  • 25
  • [ 617-84-5 ]
  • gadolinium(III) nitrate hexahydrate [ No CAS ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [Gd3(3,5-bis(3-carboxyphenyl)pyridine)4(μ-HCOO)(μ-H2O)(H2O)2(N,N-diethylformamide)]n*n(H2O) [ No CAS ]
  • 26
  • [ 617-84-5 ]
  • dysprosium(III) nitrate hexahydrate [ No CAS ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [Dy3(3,5-bis(3-carboxyphenyl)pyridine)4(μ-HCOO)(μ-H2O)(H2O)2(N,N-diethylformamide)]n*n(H2O) [ No CAS ]
  • 27
  • [ 617-84-5 ]
  • samarium(III) nitrate hexahydrate [ No CAS ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • [Sm3(3,5-bis(3-carboxyphenyl)pyridine)4(μ-HCOO)(μ-H2O)(H2O)2(N,N-diethylformamide)]n*n(H2O) [ No CAS ]
  • 28
  • copper(II) nitrate trihydrate [ No CAS ]
  • [ 1429436-06-5 ]
  • C19H11NO4(2-)*Cu(2+)*H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
56% In acetonitrile; at 120℃; for 72h; With regard to complex 1, the mixture of Cu(NO3)2·3H2O (24mg, 0.1mmol), MeCN (1mL), H2L1 (26mg, 0.08mmol), and water (4mL) was heated for 3 days under 120C in Teon-lined stainless steel container of 25mL. and at a speed of 5C/h slow cooling them to room temperature. Accordingly, blue block crystals 1·H2O were obtained that its pure yield was 56% (on the basis of H2L1). Elemental analysis: Anal. Calc. for C19H13CuNO5: N, 3.51; H, 3.29; C, 57.22. Found: N, 3.32%; H, 3.25; C, 57.21. IR (KBr, cm-1): IR (4000-400cm-1): 3825 (w), 3752 (w), 3427 (brs), 2123 (s), 1616 (s), 1366 (s), 1024 (w), 774 (s), 546 (s).
  • 29
  • cobalt(II) nitrate hexahydrate [ No CAS ]
  • [ 1429436-06-5 ]
  • [ 7732-18-5 ]
  • C19H11NO4(2-)*Co(2+)*H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
56% In acetonitrile; at 120℃; for 72h;Autoclave; With regard to the synthesis of complex 1, the mixture of Co(NO3)2*3H2O (30 mg, 0.1 mmol), MeCN (1 mL), H2L1 (26 mg, 0.08 mmol), and water (4 mL) was heated for 3 days at 120 C in a Teflonlined stainless steel container of 25 mL, and heated at a speed of 5 C/h followed by their slow cooling to room temperature. Accordingly, pink block crystals 1 were obtained with a pure yield of 56% (on the basis of H2L1). Elemental analysis calc. for C19H13CoNO5 (%): N 3.12, H 3.18, C 57.49. Found (%): N 3.32, H 3.25, C 57.21.
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