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[ CAS No. 14296-16-3 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 14296-16-3
Chemical Structure| 14296-16-3
Structure of 14296-16-3 * Storage: {[proInfo.prStorage]}
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Product Details of [ 14296-16-3 ]

CAS No. :14296-16-3 MDL No. :
Formula : C20H40Br2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 440.34 Pubchem ID :-
Synonyms :

Safety of [ 14296-16-3 ]

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Application In Synthesis of [ 14296-16-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 14296-16-3 ]

[ 14296-16-3 ] Synthesis Path-Downstream   1~7

  • 1
  • [ 2834-05-1 ]
  • [ 14296-16-3 ]
YieldReaction ConditionsOperation in experiment
54% With sodium In methanol at 20 - 30℃; for 8h; electrolysis;
With methanol; sodium Electrolysis.an Platin-Anoden;
With potassium hydroxide; ethanol Electrolysis.an Platin-Anoden;
With sodium In methanol at 45℃; for 8h; (electrolysis);
(electrolysis);
In methanol electrolysis;
With sodium hydride In methanol Electrolysis;
70 %Spectr. With pyridine; potassium hydroxide In methanol; cyclohexane; acetonitrile Electrolysis; 4.1. Kolbe-couplings with cyclohexane General procedure: Carboxylic acids (2.5 mmol) were added to electrolyte solutions (20 mL) using potassium hydroxide as a supporting electrolyte (saturated) in the presence of the cycloalkanes. The undivided reaction cell was capped with a septum equipped with platinum electrodes (10 mm×20 mm). The electrolysis was then performed at constant current. After completion of the reaction, the cycloalkane phase was concentrated under reduced pressure and the residue was purified by silica gel column chromatography using n-hexane-EtOAc to give products. The products' yields were determined by NMR.

  • 3
  • [ 627-91-8 ]
  • [ 2834-05-1 ]
  • [ 14296-16-3 ]
  • [ 41240-56-6 ]
  • [ 106-79-6 ]
YieldReaction ConditionsOperation in experiment
With sodium In methanol; water at 45 - 50℃; for 42h; (electrolysis);
  • 4
  • [ 7735-43-5 ]
  • [ 14296-16-3 ]
  • [ 92002-48-7 ]
YieldReaction ConditionsOperation in experiment
49% With hydrogen bromide In Petroleum ether for 24h; Heating;
  • 6
  • [ 42235-38-1 ]
  • [ 14296-16-3 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 62.5 percent / Red-Al / tetrahydrofuran / 3 h 2: 79.7 percent / aq. HBr; Ac2O / 5 h / Heating
Multi-step reaction with 2 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / Reflux; Inert atmosphere 2: N-Bromosuccinimide; triphenylphosphine / tetrahydrofuran / 0.5 h / 20 °C
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