Alternatived Products of [ 143-09-9 ]
Product Details of [ 143-09-9 ]
CAS No. : | 143-09-9 |
MDL No. : | |
Formula : |
C10H24ClN
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Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
193.76
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Pubchem ID : | - |
Synonyms : |
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Safety of [ 143-09-9 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 143-09-9 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Upstream synthesis route of [ 143-09-9 ]
- Downstream synthetic route of [ 143-09-9 ]
- 1
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[ 96-26-4 ]
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[ 143-09-9 ]
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[ 38993-84-9 ]
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[ 226930-96-7 ]
Yield | Reaction Conditions | Operation in experiment |
52% |
|
37-1) 5-Hydroxymethyl-1-decylimidazole The title compound was obtained in a yield of 52percent according to the same procedure as Preparation 31-1) using dihydroxyacetone and decylamine hydrochloride as starting materials. 1H NMR(CDCl3) delta0.88(t, 3H), 1.04(brs, 2H), 1.30(brs, 14H), 1.42(m, 2H), 3.68(t, 2H), 4.23(brs, 1H), 4.60(s, 2H), 6.84(s, 1H), 7.44(s, 1H) |
- 2
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[ 629-25-4 ]
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[ 156-54-7 ]
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[ 143-09-9 ]
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[ 3858-78-4 ]
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[ 10264-16-1 ]
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[ 22205-13-6 ]
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[ 551902-84-2 ]
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[ 6284-08-8 ]
- 3
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[ 629-25-4 ]
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[ 143-09-9 ]
-
[ 22205-13-6 ]
- 4
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[ 629-25-4 ]
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[ 143-09-9 ]
-
[ 3858-78-4 ]
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[ 22205-13-6 ]
-
[ 6284-08-8 ]
- 5
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[ 1984-06-1 ]
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[ 143-09-9 ]
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[ 100505-02-0 ]
Yield | Reaction Conditions | Operation in experiment |
69 %Chromat. |
With octyl 2-(N-(4,6-dimethoxy-1,3,5-triazin-2-yl)-N,N-dimethylammonio)acetate trifluoromethanesulfonate; n-butylamine hydrochloride In methanol at 25℃; for 12h; aq. phosphate buffer; Micellar solution; |
|
- 6
-
[ 1975-78-6 ]
-
[ 143-09-9 ]
Yield | Reaction Conditions | Operation in experiment |
95% |
Stage #1: n-decanenitrile With MnBr(CO)2[NH(CH2CH2P(iPr)2)2]; hydrogen; sodium t-butanolate In toluene at 120℃; for 36h; Autoclave;
Stage #2: With hydrogenchloride In diethyl ether |
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98 %Spectr. |
With hydrogenchloride; hydrogen In propan-1-ol; water at 60 - 70℃; for 3h; Flow reactor; |
|
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Stage #1: n-decanenitrile With hydrogen; C20H40MoN2O2P2; sodium triethylborohydride In tetrahydrofuran; toluene at 100℃; for 24h; Autoclave;
Stage #2: With hydrogenchloride In diethyl ether; water |
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Reference:
[1]Elangovan, Saravanakumar; Topf, Christoph; Fischer, Steffen; Jiao, Haijun; Spannenberg, Anke; Baumann, Wolfgang; Ludwig, Ralf; Junge, Kathrin; Beller, Matthias
[Journal of the American Chemical Society, 2016, vol. 138, # 28, p. 8809 - 8814]
[2]Saito, Yuki; Ishitani, Haruro; Ueno, Masaharu; Kobayashi, Shū
[ChemistryOpen, 2017, vol. 6, # 2, p. 211 - 215]
[3]Leischner, Thomas; Spannenberg, Anke; Junge, Kathrin; Beller, Matthias
[ChemCatChem, 2020, vol. 12, # 18, p. 4543 - 4549]
- 7
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[ 1975-78-6 ]
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[ 112-30-1 ]
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[ 143-09-9 ]
Yield | Reaction Conditions | Operation in experiment |
1: 68 %Spectr.
2: 12 %Spectr. |
With hydrogenchloride; water; hydrogen In propan-1-ol at 80℃; for 3h; Flow reactor; |
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