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Chemical Structure| 143814-63-5 Chemical Structure| 143814-63-5

Structure of 143814-63-5

Chemical Structure| 143814-63-5

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Product Details of [ 143814-63-5 ]

CAS No. :143814-63-5
Formula : C10H10N2O6
M.W : 254.20
SMILES Code : O=[N+](/C=C/C1=C([N+]([O-])=O)C(OC)=CC=C1OC)[O-]
MDL No. :MFCD00277337

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Application In Synthesis of [ 143814-63-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 143814-63-5 ]

[ 143814-63-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 143814-63-5 ]
  • [ 23876-39-3 ]
YieldReaction ConditionsOperation in experiment
63% With 10 wt% Pd(OH)2 on carbon; hydrogen; acetic acid; In tetrahydrofuran; at 50℃; under 7757.43 Torr; for 16h; 1,4-Dimethoxy-2-nitro-3 - [(E) -2-nitroethenyl] benzene (6.56 g)In tetrahydrofuran (100 mL)Palladium hydroxide / carbon (2 g)And acetic acid (4.2 mL)Hydrogen was added at 150 psi and stirred at 50 C. for 16 h.After cooling the reaction solution to room temperature,The solution obtained by filtration was washed with a 5% sodium bicarbonate aqueous solution.The organic layer was dried over sodium sulfate,The solvent was evaporated under reduced pressure to obtain a residue,Purification by silica gel column chromatography (hexane-ethyl acetate),4,7-Dimethoxy-1H-indole2.9 g (yield 63%) was obtained.
 

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