Home Cart 0 Sign in  
X

[ CAS No. 14504-07-5 ] {[proInfo.proName]}

,{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]}
3d Animation Molecule Structure of 14504-07-5
Chemical Structure| 14504-07-5
Chemical Structure| 14504-07-5
Structure of 14504-07-5 * Storage: {[proInfo.prStorage]}
Cart0 Add to My Favorites Add to My Favorites Bulk Inquiry Inquiry Add To Cart

Quality Control of [ 14504-07-5 ]

Related Doc. of [ 14504-07-5 ]

Alternatived Products of [ 14504-07-5 ]

Product Details of [ 14504-07-5 ]

CAS No. :14504-07-5 MDL No. :MFCD05664042
Formula : C10H10O4 Boiling Point : -
Linear Structure Formula :- InChI Key :TYAIGNOSODVIHJ-UHFFFAOYSA-N
M.W :194.18 Pubchem ID :15278258
Synonyms :

Safety of [ 14504-07-5 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P330-P363-P501 UN#:
Hazard Statements:H302-H312-H332 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 14504-07-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 14504-07-5 ]

[ 14504-07-5 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 50-85-1 ]
  • [ 108-24-7 ]
  • [ 14504-07-5 ]
YieldReaction ConditionsOperation in experiment
89% With sulfuric acid at 20℃; for 1h; Inert atmosphere; 8.B3 Example 8: Synthesis procedures B3: 4Me-NO-ASA In an inert 250 mL three-necked round bottom flask 6.00 g (39.4 mmol, 1.00 eq) 2-hydroxy-4-methylbenzoic acid and 13.1 g (159 mmol, 12.1 mL, 3.26 eq) acetic acid anhydride were mixed. To this suspension a catalytic amount (69.5 mg (990 μηιοΙ, 52.5 il, 0.03 eq)) of concentrated sulphuric acid was added. After 1 hour 83.7 mL water were added and stirring was continued for additional 13 h. The precipitate was filtered off, washed with 200 mL water. The title compound was obtained as a colourless solid in 6.79 g (34.9 mmol, 89 %).
With pyridine; diethyl ether
With quinoline
With sulfuric acid at 90℃;
Heating;
With sulfuric acid
With sulfuric acid
With phosphoric acid at 80℃; for 0.5h;
With phosphoric acid
With triethylamine In tetrahydrofuran at 20℃; Inert atmosphere; Cooling with ice;

Reference: [1]Current Patent Assignee: UNIVERSITÄT ZU KÖLN - WO2015/44177, 2015, A1 Location in patent: Page/Page column 25
[2]Chuit; Bolsing [Bulletin de la Societe Chimique de France, 1906, vol. <3> 35, p. 142]
[3]Current Patent Assignee: BAYER AG - DE386679, 1923, C [Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 1239][Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 1239]
[4]Chuit; Bolsing [Bulletin de la Societe Chimique de France, 1906, vol. <3> 35, p. 142]
[5]Current Patent Assignee: BAYER AG - DE386679, 1923, C [Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 1239][Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 1239]
[6]Anschuetz; Gross [Chemische Berichte, 1944, vol. 77/79, p. 644,647]
[7]Yamamoto, Satoshi; Hashiguchi, Shohei; Miki, Shokyo; Igata, Yumiko; Watanabe, Toshifumi; Shiraishi, Mitsuru [Chemical and Pharmaceutical Bulletin, 1996, vol. 44, # 4, p. 734 - 745]
[8]Yu, Kuo-Long; Ruediger, Edward; Luo, Guangxiang; Cianci, Christopher; Danetz, Stephanie; Tiley, Laurence; Trehan, Ashok K.; Monkovic, Ivo; Pearce, Bradley; Martel, Alain; Krystal, Mark; Meanwell, Nicholas A. [Bioorganic and Medicinal Chemistry Letters, 1999, vol. 9, # 15, p. 2177 - 2180]
[9]Spencer, Jeffrey R; McGee, Danny; Allen, Darin; Katz, Bradley A; Luong, Christine; Sendzik, Martin; Squires, Neil; Mackman, Richard L [Bioorganic and Medicinal Chemistry Letters, 2002, vol. 12, # 15, p. 2023 - 2026]
[10]Shrestha, Suja; Bhattarai, Bharat Raj; Kafle, Bhooshan; Lee, Keun-Hyeung; Cho, Hyeongjin [Bioorganic and Medicinal Chemistry, 2008, vol. 16, # 18, p. 8643 - 8652]
[11]Liu, Yanfei; Long, Shuo; Zhang, Shanshan; Tan, Yifu; Wang, Ting; Wu, Yuwei; Jiang, Ting; Liu, Xiaoqin; Peng, Dongming; Liu, Zhenbao [RSC Advances, 2021, vol. 11, # 29, p. 17611 - 17621]
[12]Baecker, Daniel; Sagasser, Jessica; Karaman, Serhat; Hörmann, Anton Amadeus; Gust, Ronald [Archiv der Pharmazie, 2022, vol. 355, # 2]
  • 2
  • [ 14504-07-5 ]
  • [ 49667-22-3 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: oxalyl chloride / dimethylformamide; tetrahydrofuran / Ambient temperature 2: conc. aq. NH3 / tetrahydrofuran / Ambient temperature
Same Skeleton Products
Historical Records