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Chemical Structure| 146519-40-6 Chemical Structure| 146519-40-6

Structure of 146519-40-6

Chemical Structure| 146519-40-6

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Product Details of [ 146519-40-6 ]

CAS No. :146519-40-6
Formula : C8H7N3O
M.W : 161.16
SMILES Code : CC(C1=CC=C(N=NN2)C2=C1)=O

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Application In Synthesis of [ 146519-40-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 146519-40-6 ]

[ 146519-40-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 5780-37-0 ]
  • [ 3325-11-9 ]
  • [ 96042-30-7 ]
  • [ 146519-40-6 ]
YieldReaction ConditionsOperation in experiment
5-Acetyl-1H-Benzotriazole [25] The ketone was prepared in the same manner as the benzotriazole aldehyde from <strong>[3325-11-9]5-aminobenzotriazole</strong> and acetaldoxime. Column chromatography of the crude ketone using DCM and eluding with MeOH (0-10percent) afforded the ketone in 11percent yield. Rf [A] 0.3; deltaH(400MHz; Acetone-d6) 2.68 (3H, s, CH3), 7.92 (1H, d, J 8.7, Ar-H), 8.07 (1H, d, J 8.7 Ar-H), 8.62 (1H, s, Ar-H); m/z (FAB-HR) 162.06674 [(M+H)+ calc. for C8H8N3O 162.06682]. The hydrazone of the ketone was prepared from 2,4DNPH to afford an orange solid.
 

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