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Chemical Structure| 1467060-89-4 Chemical Structure| 1467060-89-4

Structure of 1467060-89-4

Chemical Structure| 1467060-89-4

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Product Details of [ 1467060-89-4 ]

CAS No. :1467060-89-4
Formula : C13H16BrNO3
M.W : 314.18
SMILES Code : O=C1N(CCCOC2=CC=C(Br)C=C2)CCOC1
MDL No. :MFCD28133785

Safety of [ 1467060-89-4 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P261-P302+P352-P305+P351+P338

Application In Synthesis of [ 1467060-89-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1467060-89-4 ]

[ 1467060-89-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 109-11-5 ]
  • [ 7497-87-2 ]
  • [ 1467060-89-4 ]
YieldReaction ConditionsOperation in experiment
35% With sodium hydride; In N,N-dimethyl-formamide; at 75℃; for 5h; To a mixture of 1-bromo-4-(3-bromopropoxy)benzene (300 mg, 1.02 mmol) and <strong>[109-11-5]morpholin-3-one</strong> (100 mg, 1.02 mmol) in DMF (6 mL) was added NaH (365 mg, 1.10 mmol). The mixture was stirred at 75 C. for 5 hours. The mixture was poured into ethyl acetate and washed with water. The organic phase was dried over sodium sulfate, filtered, and concentrated to give the title compound (100 mg, 35%) as a yellow oil.
 

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