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Chemical Structure| 148870-56-8 Chemical Structure| 148870-56-8

Structure of 148870-56-8

Chemical Structure| 148870-56-8

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Product Details of [ 148870-56-8 ]

CAS No. :148870-56-8
Formula : C12H17NO2
M.W : 207.27
SMILES Code : CNCC1C2=CC(OC)=C(OC)C=C2C1

Safety of [ 148870-56-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330

Application In Synthesis of [ 148870-56-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 148870-56-8 ]

[ 148870-56-8 ] Synthesis Path-Downstream   1~2

  • 2
  • [ 35202-54-1 ]
  • [ 74-89-5 ]
  • [ 148870-56-8 ]
YieldReaction ConditionsOperation in experiment
91% With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; at 20℃; for 16h; 4.5-Dimethoxy-l-cyano-benzo cyclobutane (50gm) was dissolved in a Flask containing Tetrahydrofuran (750 ml) at room temperature followed by the addition of 40% of Monomethyl amine (40gm) solution in Tetrahydrofuran (250 ml) and 10% Pd/C of 50% wet (l5gm). Hydrogen 4-5kgswas applied and the reaction was stirred for 16 hours at room temperature. After completion of reaction, the resultant mass was filtered through Hyflow bed and distilled the solvent under vacuum to obtain the crude 3,4-Dimethoxy n-methyl bicyclo [4.2.0] octa-l,3,5-triene-7- methanamine. (0122) Recovery of Palladium Carbon: l3gms (0123) Yield: 91%
 

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