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Chemical Structure| 150215-07-9 Chemical Structure| 150215-07-9

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Chemical Structure| 150215-07-9

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Product Details of [ 150215-07-9 ]

CAS No. :150215-07-9
Formula : C8H11N3O4S
M.W : 245.26
SMILES Code : CCOC(=O)NC1=NC(CC(=O)OC)=NS1
MDL No. :MFCD11112136

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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 150215-07-9 ]

[ 150215-07-9 ] Synthesis Path-Downstream   1~2

  • 2
  • [ 541-41-3 ]
  • [ 32326-25-3 ]
  • [ 150215-07-9 ]
YieldReaction ConditionsOperation in experiment
78.9% In acetonitrile; Example 2 A suspension of ethyl chloroformate (124 mul; 1.29 mmol) and potassium thiocyanate (136 mg; 1.40 mmol) in acetonitrile (1.08 ml) was treated with <strong>[32326-25-3]<strong>[32326-25-3]3-amino-5-methoxyisoxazol</strong>e</strong> (123 mg; 1.08 mmol) in the same manner as in Example 1 except that ethyl chloroformate was substituted for methyl chloroformate to give methyl 2-(5-ethoxycarbonylamino-1,2,4-thiadiazol-3yl)acetate (209 mg; yield 78.9%). m.p. 110-112 C. (MeOH) NMR delta (CDCl3): 1.38(3H.t.CH3) 3.73(3H.s.COOCH3) 3.97(2H.s.CH2 COOCH3) 4.39(2H.q. CH2) 10.45(1H.bs.NH) IR(CHCl3)cm-1: 3406, 1732, 1564. Anal. Calcd. for C8 H11 N3 O4 S: C,39.18; H, 4.52; N, 17.13(%). Found: C,39.16; H,4.40; N,17.18(%).
 

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