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CAS No. : | 150319-83-8 | MDL No. : | MFCD11501071 |
Formula : | C9H12ClNO2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | OOGVJPZOIXNNHQ-UHFFFAOYSA-N |
M.W : | 201.65 | Pubchem ID : | 44119610 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
96.8% | With thionyl chloride In methanol | A. 3-Amino phenylacetic acid methylester hydrochloride A suspension of 3-amino phenylacetic acid (5.0 g, 33 mmol) in methanol (50 ml) at 0° C. under argon was slowly treated with thionyl chloride (19.4 g, 165 mmol). After completion of addition, the reaction mixture was allowed to warm up to room temperature and stirred for 16 hours. The solvent was evaporated and the residue was triturated with ethyl ether to give 3-amino phenylacetic acid methylester hydrochloride (5.3 g, 96.8percent) as a colorless solid. 1 H NMR (CDCl3) δ 10.6 (s, 2 H), 7.42 (m, 4 H), 3.68 (s, 3 H). 3.66 (s,2 H); 13 C NMR (CDCl3) 172.5, 137.3, 133.1, 131.2, 130.8, 125.9, 123.7, 53.5, 41.5. |
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