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Chemical Structure| 15136-26-2 Chemical Structure| 15136-26-2

Structure of Cyclo(Ala-Val)
CAS No.: 15136-26-2

Chemical Structure| 15136-26-2

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Product Details of [ 15136-26-2 ]

CAS No. :15136-26-2
Formula : C8H14N2O2
M.W : 170.21
SMILES Code : O=C([C@H](C(C)C)N1)N[C@@H](C)C1=O
MDL No. :MFCD24549359

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Application In Synthesis of [ 15136-26-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 15136-26-2 ]

[ 15136-26-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1115-74-8 ]
  • [ 15136-26-2 ]
YieldReaction ConditionsOperation in experiment
99% at 200℃; for 0.5h; <strong>[1115-74-8]L-valyl-L-alanine</strong> (260 mg, 1.381 mmol) was taken in a 5 mL vial and heated to 200 C for 30 minutes. The solid collected on the side walls of the vial to yield the (3S,6S)-3-isopropyl-6-methylpiperazine-2,5-dione (235 mg, 99 % yield) as an off-white solid. LCMS: m/z = 171.2 (M+H); rt 0.22 min; Column-Kinetex XB-C18 (75X3 mm-2.6 ^m), Mobile phase A: 10 mM ammonium formate in water:acetonitrile (98:2), Mobile phase B: 10 mM ammonium formate in water:acetonitrile (2:98).
 

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