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Chemical Structure| 15217-42-2 Chemical Structure| 15217-42-2

Structure of 15217-42-2

Chemical Structure| 15217-42-2

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Product Details of [ 15217-42-2 ]

CAS No. :15217-42-2
Formula : C6H4N3Na
M.W : 141.11
SMILES Code : C12=CC=CC=C1[N-]N=N2.[Na+]

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Application In Synthesis of [ 15217-42-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 15217-42-2 ]

[ 15217-42-2 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 506-68-3 ]
  • [ 15217-42-2 ]
  • [ 15328-32-2 ]
  • [ 28992-50-9 ]
  • 2
  • [ 626-44-8 ]
  • [ 15217-42-2 ]
  • C24H15N9 [ No CAS ]
YieldReaction ConditionsOperation in experiment
73% With copper(l) iodide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; at 80℃; for 12h;Inert atmosphere; <strong>[626-44-8]1,3,5-triiodobenzene</strong> (22.8 g, 0.05 mol) under nitrogen protection,Pd(dppf)Cl2.CH2Cl2 (2.0g, 0.0025mol) and CuI (10.0g, 0.052mol), isopropylamine (200ml) were added to tetrahydrofuran (500ml), sodium benzotriazole (22.5g, 0.16mol) The mixture was slowly added, and the mixture was heated to 80 ° C and stirred for 12 hours. TLC showed the end of the reaction, and a silica gel column (PE/EA = 2/1 to 1/1) afforded Compound 11 (15.6 g, yield 73percent).
 

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