Structure of 152270-00-3
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The BI-3802 was designed by Boehringer Ingelheim and could be obtained free of charge through the Boehringer Ingelheim open innovation portal opnMe.com, associated with its negative control.
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Batch number can be found on the product's label following the word 'Batch'.
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| CAS No. : | 152270-00-3 |
| Formula : | C34H54O2 |
| M.W : | 494.79 |
| SMILES Code : | O(C1C=C(C(=CC=1C#C)OCCCCCCCCCCCC)C#C)CCCCCCCCCCCC |
| MDL No. : | N/A |
| InChI Key : | WWYFSQMGZADESA-UHFFFAOYSA-N |
| Pubchem ID : | 15429803 |
| GHS Pictogram: |
|
| Signal Word: | Warning |
| Hazard Statements: | H302-H315-H319-H335 |
| Precautionary Statements: | P261-P280-P301+P312-P302+P352-P305+P351+P338 |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.


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[ 152270-00-3 ]
| Yield | Reaction Conditions | Operation in experiment |
|---|---|---|
| 75% | With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20℃; for 0.5h;Darkness; | Compound 14 (0.21 g, 3.29 × 10 -4 mol) was dissolved in THF (5 mL),Tetrabutylammonium fluoride (TBAF) (0.79 mL, 7.89 × 10 -4 mol) was added to the solution,The mixture was stirred at room temperature under light shielding for 30 minutes. After the reaction,The solvent was distilled off under reduced pressure,Purification was performed twice by silica gel column chromatography (CH2Cl2: hexane = 1: 3).To give Compound 15 as a pale yellow solid (yield 0.12 g, 75.0%).). |