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[ CAS No. 1530-32-1 ]

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Chemical Structure| 1530-32-1
Chemical Structure| 1530-32-1
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CAS No. :1530-32-1 MDL No. :MFCD00011838
Formula : C20H20BrP Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W :371.25 g/mol Pubchem ID :73727
Synonyms :

Safety of [ 1530-32-1 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P280-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H312-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 1530-32-1 ]

  • Upstream synthesis route of [ 1530-32-1 ]
  • Downstream synthetic route of [ 1530-32-1 ]

[ 1530-32-1 ] Synthesis Path-Upstream   1~15

  • 1
  • [ 4460-86-0 ]
  • [ 1530-32-1 ]
  • [ 5273-86-9 ]
  • [ 2883-98-9 ]
Reference: [1] Organic Preparations and Procedures International, 2007, vol. 39, # 5, p. 514 - 517
[2] Organic Preparations and Procedures International, 2009, vol. 41, # 2, p. 152 - 155
[3] Arkivoc, 2010, vol. 2010, # 2, p. 71 - 96
  • 2
  • [ 4460-86-0 ]
  • [ 1530-32-1 ]
  • [ 5273-86-9 ]
  • [ 2883-98-9 ]
  • [ 80423-94-5 ]
Reference: [1] Organic Preparations and Procedures International, 2007, vol. 39, # 5, p. 514 - 517
  • 3
  • [ 74-96-4 ]
  • [ 603-35-0 ]
  • [ 1530-32-1 ]
YieldReaction ConditionsOperation in experiment
91.8% for 10 h; Reflux In a 1500 ml reaction flask, 54 g (0.5 mol) of ethyl bromide and210 g (0.8 mol) of triphenylphosphine and 1000 ml of toluene were added,Heated to reflux with stirring for 10 hours, the reaction was cooled to 50 ° C,A large amount of solid precipitated, suction filtered, the filter cake was washed with toluene (50ml * 3 times)The solid was dried in a vacuum oven at 50 ° C,Ethyl triphenylphosphonium bromide 170.4g, yield 91.8percent
Reference: [1] Journal of Fluorine Chemistry, 2002, vol. 113, # 2, p. 177 - 183
[2] Pharmazie, 1999, vol. 54, # 1, p. 26 - 30
[3] Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989, vol. <2> 38, # 12, p. 2553 - 2556[4] Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989, vol. <2> 38, # 12, p. 2789 - 2792
[5] Journal of the American Chemical Society, 1980, vol. 102, p. 2437
[6] Patent: CN106632340, 2017, A, . Location in patent: Paragraph 0024; 0025
[7] Phosphorus, Sulfur and Silicon and the Related Elements, 2008, vol. 183, # 5, p. 1188 - 1208
[8] Organometallics, 2014, vol. 33, # 14, p. 3792 - 3803
[9] Organometallics, 2018, vol. 37, # 10, p. 1526 - 1533
[10] Journal of the American Chemical Society, 2012, vol. 134, # 22, p. 9225 - 9239
[11] Journal of Organic Chemistry, 2016, vol. 81, # 24, p. 12084 - 12090
[12] Justus Liebigs Annalen der Chemie, 1967, vol. 707, p. 120 - 129
[13] J. Gen. Chem. USSR (Engl. Transl.), 1963, vol. 33, # 6, p. 1809 - 1812[14] Zhurnal Obshchei Khimii, 1963, vol. 33, # 6, p. 1860 - 1864
[15] Journal of Organic Chemistry, 1958, vol. 23, p. 1245
[16] Justus Liebigs Annalen der Chemie, 1957, vol. 606, p. 1,16
[17] Justus Liebigs Annalen der Chemie, 1961, vol. 646, p. 65 - 77
[18] Zeitschrift fuer Chemie (Stuttgart, Germany), 1990, vol. 30, # 6, p. 193 - 204
[19] Applied Catalysis A: General, 2014, vol. 470, p. 183 - 188
[20] Chemistry - A European Journal, 2015, vol. 21, # 44, p. 15769 - 15784
[21] Organic Letters, 2016, vol. 18, # 3, p. 504 - 507
[22] Advanced Synthesis and Catalysis, 2016, vol. 358, # 11, p. 1731 - 1735
[23] Bioconjugate Chemistry, 2017, vol. 28, # 2, p. 590 - 599
[24] Patent: CN108191915, 2018, A, . Location in patent: Paragraph 0034; 0039
  • 4
  • [ 1754-88-7 ]
  • [ 1530-32-1 ]
  • [ 66070-22-2 ]
  • [ 66070-35-7 ]
Reference: [1] Tetrahedron Letters, 1987, vol. 28, # 50, p. 6317 - 6320
  • 5
  • [ 64-17-5 ]
  • [ 603-35-0 ]
  • [ 1530-32-1 ]
Reference: [1] Phosphorus, Sulfur and Silicon and the Related Elements, 1990, vol. 48, # 1-4, p. 279 - 280
  • 6
  • [ 774-48-1 ]
  • [ 6399-81-1 ]
  • [ 1530-32-1 ]
  • [ 100-52-7 ]
Reference: [1] Arkivoc, 2013, vol. 2013, # 3, p. 98 - 108
  • 7
  • [ 2689-62-5 ]
  • [ 555-16-8 ]
  • [ 40277-76-7 ]
  • [ 1530-32-1 ]
Reference: [1] Synthetic Communications, 1982, vol. 12, # 6, p. 469 - 476
  • 8
  • [ 108-86-1 ]
  • [ 20472-49-5 ]
  • [ 1530-32-1 ]
  • [ 2751-90-8 ]
  • [ 3878-45-3 ]
Reference: [1] Journal of Organometallic Chemistry, 1980, vol. 185, # 2, p. 283 - 296
  • 9
  • [ 774-48-1 ]
  • [ 6399-81-1 ]
  • [ 1530-32-1 ]
Reference: [1] Justus Liebigs Annalen der Chemie, 1967, vol. 709, p. 105 - 112
  • 10
  • [ 603-35-0 ]
  • [ 3400-55-3 ]
  • [ 1530-32-1 ]
Reference: [1] Zeitschrift fuer Chemie (Stuttgart, Germany), 1968, vol. 8, p. 184
  • 11
  • [ 16258-78-9 ]
  • [ 1530-32-1 ]
  • [ 130222-63-8 ]
Reference: [1] Journal of Chemical Research, Miniprint, 1990, # 6, p. 1349 - 1372
  • 12
  • [ 603-35-0 ]
  • [ 925669-95-0 ]
  • [ 1530-32-1 ]
  • [ 126443-67-2 ]
Reference: [1] Bulletin de la Societe Chimique de France, 1989, # 4, p. 477 - 483
  • 13
  • [ 603-35-0 ]
  • [ 21490-63-1 ]
  • [ 1530-32-1 ]
  • [ 126443-67-2 ]
Reference: [1] Bulletin de la Societe Chimique de France, 1989, # 4, p. 477 - 483
  • 14
  • [ 108-86-1 ]
  • [ 20472-49-5 ]
  • [ 1530-32-1 ]
  • [ 2751-90-8 ]
  • [ 3878-45-3 ]
Reference: [1] Journal of Organometallic Chemistry, 1980, vol. 185, # 2, p. 283 - 296
  • 15
  • [ 1530-32-1 ]
  • [ 93205-71-1 ]
  • [ 96184-40-6 ]
Reference: [1] Molecular Crystals and Liquid Crystals (1969-1991), 1985, vol. 131, p. 109 - 124
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