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Chemical Structure| 153877-53-3 Chemical Structure| 153877-53-3

Structure of 153877-53-3

Chemical Structure| 153877-53-3

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Product Details of [ 153877-53-3 ]

CAS No. :153877-53-3
Formula : C13H10F2O
M.W : 220.21
SMILES Code : OC(C1=CC=C(F)C=C1)C2=CC=CC=C2F

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Application In Synthesis of [ 153877-53-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 153877-53-3 ]

[ 153877-53-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 342-25-6 ]
  • [ 153877-53-3 ]
YieldReaction ConditionsOperation in experiment
97.8% With sodium tetrahydroborate; In ethanol; at 20℃; for 2h; (1) (2-Fluorophenyl)(4-fluorophenyl)methanol To a solution (100 ML) of <strong>[342-25-6]2,4'-difluorobenzophenol</strong> (10.0 g, 45.8 mmol) in ethanol was added sodium borohydride (867 mg, 22.9 mmol), the mixture was stirred at room temperature for 2 hours, and the solvent was distilled off under reduced pressure.. The residue was poured into water, and was extracted with ethyl acetate.. The extracted solution was washed with water, was dried with anhydrous magnesium sulfate, and the solvent was distilled off under reduced pressure, to obtain the titled compound as oil. 9.88 g (97.8%) 1H-NMR (CDCl3) delta; 2.32 (1H, d, J = 4.0 Hz), 5.83 (1H, d, J = 4.0 Hz), 6.95 to 7.53 (8H, m)
 

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