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Chemical Structure| 154744-75-9 Chemical Structure| 154744-75-9

Structure of 154744-75-9

Chemical Structure| 154744-75-9

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Product Details of [ 154744-75-9 ]

CAS No. :154744-75-9
Formula : C3H10N2O3S
M.W : 154.19
SMILES Code : O=S(N)(NCCOC)=O

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Application In Synthesis of [ 154744-75-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 154744-75-9 ]

[ 154744-75-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 68797-61-5 ]
  • [ 154744-75-9 ]
  • C7H10BrClN4O3S [ No CAS ]
YieldReaction ConditionsOperation in experiment
61.56% 4) at room temperature,Compound D (1.12 g, 7.24 mmol) and potassium t-butoxide (2.22 g, 19.75 mmol) were added to dimethyl sulfoxide (20.00 mL).The reaction mixture was stirred at room temperature for 0.5 hours.Subsequently, <strong>[68797-61-5]5-bromo-4,6-dichloropyrimidine</strong> (1.50 g, 6.58 mmol) was added to the above reaction solution.The reaction mixture was stirred at room temperature for 6 hours.After completion of the reaction, water (100 mL) was added, and the mixture was adjusted to pH 6 with 1M diluted hydrochloric acid, and ethyl acetate (100 mL x 3).The organic layer was combined, washed with brine (100 mL) Volume ratio),The title compound E (yellow solid, 1.40 g, yield: 61.56%) was obtained.
 

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