There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.
Type | HazMat fee for 500 gram (Estimated) |
Excepted Quantity | USD 0.00 |
Limited Quantity | USD 15-60 |
Inaccessible (Haz class 6.1), Domestic | USD 80+ |
Inaccessible (Haz class 6.1), International | USD 150+ |
Accessible (Haz class 3, 4, 5 or 8), Domestic | USD 100+ |
Accessible (Haz class 3, 4, 5 or 8), International | USD 200+ |
Structure of 16068-37-4
*Storage: {[sel_prStorage]}
*Shipping: {[sel_prShipping]}
The BI-3802 was designed by Boehringer Ingelheim and could be obtained free of charge through the Boehringer Ingelheim open innovation portal opnMe.com, associated with its negative control.
4.5
*For Research Use Only !
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Search for reports by entering the product batch number.
Batch number can be found on the product's label following the word 'Batch'.
Search for reports by entering the product batch number.
Batch number can be found on the product's label following the word 'Batch'.
Search for reports by entering the product batch number.
Batch number can be found on the product's label following the word 'Batch'.
Search for reports by entering the product batch number.
Batch number can be found on the product's label following the word 'Batch'.
Search for reports by entering the product batch number.
Batch number can be found on the product's label following the word 'Batch'.
CAS No. : | 16068-37-4 |
Formula : | C14H34O6Si2 |
M.W : | 354.59 |
SMILES Code : | CCO[Si](OCC)(OCC)CC[Si](OCC)(OCC)OCC |
MDL No. : | MFCD00239362 |
InChI Key : | IZRJPHXTEXTLHY-UHFFFAOYSA-N |
Pubchem ID : | 85266 |
GHS Pictogram: |
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Signal Word: | Danger |
Hazard Statements: | H301-H312-H372-H412 |
Precautionary Statements: | P264-P270-P280-P301+P310-P302+P352-P312-P330-P362+P364-P405-P501 |
Class: | 6.1 |
UN#: | 2810 |
Packing Group: | Ⅲ |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
87% | at 60 - 120℃; for 3 h; Inert atmosphere | Weigh 468g of ethanol into the constant pressure dropping funnel, while 500gbis (trichloro) silylethane into a three-neck flask, heated in an oil bath, while the temperature rose to at 60 , open magnetic stirrer was slowly added dropwise 1 / 3 parts of ethanol, while nitrogen gas bubbling hydrogen chloride off reaction, the dropwise addition 40min; temperature was raised to 90 deg.] C, was added dropwise 1/3 parts ethanol, 50min dropwise addition, reaction was continued for 30min; temperature was raised to 120 deg.] C, continue the remaining solution of ethanol, 60min dropping end. After the addition, continue nitrogen until the solution Cl- content of less than 1percent, the reaction was stopped. Was added dropwise a solution of sodium ethoxide was neutralized, until the solution was neutral, the solution was filtered to remove salt wherein the resulting liquid was filtered at a vacuum degree of 0.08Mpa ~ 0.098Mpa, a temperature of 120 ~ 160 distillation under reduced pressure to give the product as a colorless bis (triethoxysilyl) ethane silicon, the final quantity was 522 g, 87percent yield of the final product. |