Home Cart Sign in  
Chemical Structure| 16076-61-2 Chemical Structure| 16076-61-2

Structure of 16076-61-2

Chemical Structure| 16076-61-2

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 16076-61-2 ]

CAS No. :16076-61-2
Formula : C13H22O3
M.W : 226.31
SMILES Code : O=C(OCC)CCCC(C1CCCCC1)=O
MDL No. :MFCD01320319

Safety of [ 16076-61-2 ]

Application In Synthesis of [ 16076-61-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 16076-61-2 ]

[ 16076-61-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 16076-61-2 ]
  • [ 100063-22-7 ]
  • [ 1356457-45-8 ]
YieldReaction ConditionsOperation in experiment
15% With phenylsilane; dibutyltin chloride; In 1,4-dioxane; at 120℃; for 2h;Microwave irradiation; A flask was charged with 3-amino-5-phenyl-thiophene-2-carboxylic acid methyl ester (515 mg, 2.2 mmol, 1 .0 equiv), 5-cyclohexyl-5-oxo-pentanoic acid ethyl ester (500 mg, 2.2 mmol, 1 .0 equiv), phenyl silane (240 mg, 2.2 mmol, 1 .0 equiv), dibutyltin dichloride (67 mg, 0.22 mmol, 0.1 equiv) and dioxane (2.0 mL). The resulting solution was heated at 120 C with microwave for 2 hours. The solution was then concentrated and the residue was purified by silica gel column chromatography, EtOAc/heptane 5% to 40%, to give oil that contained starting material. The material was further purified with silica gel column chromotography, EtOH/DCM 2%to 10% to give product 150 mg (yield 15%).
 

Historical Records

Technical Information

Categories