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[ CAS No. 163295-76-9 ] {[proInfo.proName]}

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3d Animation Molecule Structure of 163295-76-9
Chemical Structure| 163295-76-9
Chemical Structure| 163295-76-9
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Product Details of [ 163295-76-9 ]

CAS No. :163295-76-9 MDL No. :MFCD07778384
Formula : C8H9ClO3S Boiling Point : -
Linear Structure Formula :- InChI Key :HIBDAKCYUPOBNR-UHFFFAOYSA-N
M.W : 220.67 Pubchem ID :23211153
Synonyms :

Safety of [ 163295-76-9 ]

Signal Word:Danger Class:8
Precautionary Statements:P260-P264-P270-P271-P280-P301+P330+P331-P303+P361+P353-P304+P340-P305+P351+P338-P310-P363-P403+P233-P405-P501 UN#:3261
Hazard Statements:H302-H335-H314 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 163295-76-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 163295-76-9 ]

[ 163295-76-9 ] Synthesis Path-Downstream   1~11

  • 1
  • sodium; (3-methoxy-phenyl)-methanesulfonate [ No CAS ]
  • [ 163295-76-9 ]
YieldReaction ConditionsOperation in experiment
With thionyl chloride In N,N-dimethyl-formamide at 20℃; for 4h;
  • 2
  • [ 163295-76-9 ]
  • [ 2595-05-3 ]
  • [ 872676-56-7 ]
YieldReaction ConditionsOperation in experiment
1.51 g With pyridine In ethyl acetate for 24h;
  • 3
  • [ 163295-76-9 ]
  • (R)-3-[(3aR,5R,6R,6aR)-5-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxysulfonyl]-3-(3-methoxy-phenyl)-propionic acid methyl ester [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: 1.51 g / pyridine / ethyl acetate / 24 h 2.1: n-BuLi / tetrahydrofuran; hexane / 0.75 h / -95 °C 2.2: tetrahydrofuran; hexane / 17 h / -95 - -78 °C
  • 4
  • [ 163295-76-9 ]
  • (S)-3-[(3aR,5R,6R,6aR)-5-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxysulfonyl]-3-(3-methoxy-phenyl)-propionic acid methyl ester [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: 1.51 g / pyridine / ethyl acetate / 24 h 2.1: n-BuLi / tetrahydrofuran; hexane / 0.75 h / -95 °C 2.2: tetrahydrofuran; hexane / 17 h / -95 - -78 °C
YieldReaction ConditionsOperation in experiment
68%
  • 6
  • [ 163295-76-9 ]
  • [ 771-60-8 ]
  • [ 1298109-24-6 ]
YieldReaction ConditionsOperation in experiment
Stage #1: (3-methoxyphenyl)methanesulfonyl chloride With pyridine; dmap at 20℃; for 0.25h; Stage #2: 2,3,4,5,6-pentafluoroaniline at 20℃;
  • 7
  • [ 163295-76-9 ]
  • [ 771-60-8 ]
  • [ 1298109-35-9 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: pyridine; dmap / 0.25 h / 20 °C 1.2: 20 °C 2.1: N-Ac-Leu; silver(I) acetate; palladium diacetate; N,N-dimethyl-formamide / dichloromethane / 36 h / 80 °C / Sealed tube; Under air
  • 8
  • [ 163295-76-9 ]
  • [ 328-74-5 ]
  • N-(3,5-bis(trifluoromethyl)phenyl)-1-(3-methoxyphenyl)methanesulfonamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
95% With triethylamine In dichloromethane at 20℃; for 12h;
  • 9
  • [ 163295-76-9 ]
  • [ 328-74-5 ]
  • methyl 3'-((N-(3,5-bis(trifluoromethyl)phenyl)sulfamoyl)methyl)-5'-methoxy-[1,1'-biphenyl]-2-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: triethylamine / dichloromethane / 12 h / 20 °C 2: palladium diacetate; 2-carbomethoxynorbornene; silver(I) acetate; isoquinoline / 1,2-dichloro-ethane / 24 h / 100 °C / Sealed tube
  • 10
  • [ 874-98-6 ]
  • [ 163295-76-9 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: sodium sulfite / water; acetone / 16 h / 90 °C 2: oxalyl dichloride; N,N-dimethyl-formamide / N,N-dimethyl-formamide; dichloromethane / 2.5 h / -20 - 20 °C
  • 11
  • (3-methoxyphenyl)methanesulfonic acid [ No CAS ]
  • [ 163295-76-9 ]
YieldReaction ConditionsOperation in experiment
65% With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane; N,N-dimethyl-formamide at -20 - 20℃; for 2.5h; xxi.b (3-Methoxyphenyl)methanesulfonyl chloride I48 To a stirred solution of (3-methoxyphenyl)methanesulfonic acid I47a (636 mg, 3.15 mmol) in DCM (25 mL) was added DMF (5 drops) and the mixture was cooled to -20 °C. Oxalyl chloride (2.7 mL, 31.4 mmol) was added and the mixture was stirred at -20 °C for 30 min, then allowed to warm to room temperature and stirred for 2 h. DCM (20 mL) was added and the mixture was washed with water and brine. The organic layer was dried over Na2S04, filtered and concentrated to give the title compound (450 mg, 65%) as a yellow oil, which was used in the next step without further purification. LCMS-A (ES-API): Rt 0.95 min; m/z 237.8 [M+Na]+ (LCMS sample treated with MeNH2 to give 1 -(3-methoxyphenyl)-N- methylmethanesulfonamide, exact mass: 215.06).
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