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Chemical Structure| 1641-36-7 Chemical Structure| 1641-36-7

Structure of 1641-36-7

Chemical Structure| 1641-36-7

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Product Details of [ 1641-36-7 ]

CAS No. :1641-36-7
Formula : C6H15NO2
M.W : 133.19
SMILES Code : CCCCN.CC(O)=O
MDL No. :N/A

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Application In Synthesis of [ 1641-36-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1641-36-7 ]

[ 1641-36-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1641-36-7 ]
  • [ 140-53-4 ]
  • [ 20101-92-2 ]
  • [ 115601-10-0 ]
YieldReaction ConditionsOperation in experiment
7%; 83% General Procedure for the synthesis of imides: 1 mmol of Tf2O (0.16 mL) was added to 1 mmol of ionic liquid at 0 C, and the mixture was stirred for 5 min at room temperature. Then, 1 mmol of the nitrile was added and the mixture was heated at 60 C. After 1 h, NaHCO3 (2%, 5 mL) was added and the mixture was extracted with EtOAc (2 × 5 mL). The organic layer was dried over Na2SO4 and evaporated. The crude product was purified by column chromatography using EtOAc/n-hexane (2:8) as eluent to afford the desired imide. Spectral and analytical data for new compounds:
 

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