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Chemical Structure| 170811-08-2 Chemical Structure| 170811-08-2

Structure of 170811-08-2

Chemical Structure| 170811-08-2

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Product Details of [ 170811-08-2 ]

CAS No. :170811-08-2
Formula : C15H22O4S
M.W : 298.40
SMILES Code : O=S(C1=CC=C(C)C=C1)(OC[C@H]2CC[C@H](CO)CC2)=O

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Application In Synthesis of [ 170811-08-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 170811-08-2 ]

[ 170811-08-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 3236-48-4 ]
  • [ 98-59-9 ]
  • [ 170811-08-2 ]
YieldReaction ConditionsOperation in experiment
With triethylamine; In dichloromethane; at -20 - 20℃; for 10h; Step 2: 4-Toluenesulfonyl chloride (742.5 g, 3.75 mol) was added to a solution of trans-cyclohexane-1,4-diyldimethanol (500 g, 4.17 mol) and Et3N (695 g, 5 mol) in DCM (6000 mL) at -20° C. The mixture was stirred at room temperature for 10 h and then quenched with water (10 L). The organic layer was separated, the aqueous layer was extracted with DCM (2*3 L), and the combined organic layer was dried over sodium sulfate, filtered, and concentrated in vacuo to give trans-4-(hydroxymethyl)cyclohexylmethyl 4-methylbenzenesulfonate as a yellow oil.
 

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