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Chemical Structure| 174621-50-2 Chemical Structure| 174621-50-2

Structure of 174621-50-2

Chemical Structure| 174621-50-2

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Product Details of [ 174621-50-2 ]

CAS No. :174621-50-2
Formula : C17H15NO2
M.W : 265.31
SMILES Code : CCOC(C1=CC=C(N2C=CC3=CC=CC=C32)C=C1)=O

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Application In Synthesis of [ 174621-50-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 174621-50-2 ]

[ 174621-50-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 174621-50-2 ]
  • [ 177420-64-3 ]
  • ethyl 4-{3-[2-bromo-6-(trifluoromethyl)benzoyl]-1H-indol-1-yl}benzoate [ No CAS ]
YieldReaction ConditionsOperation in experiment
0.15 g 2-Bromo-6- (trifluoromethyl) benzoic acid (0.203 g)Was dissolved in dichloromethane (3 mL)Under ice cooling, oxalyl chloride (0.0710 mL)And a catalytic amount of N, N-dimethylformamide were added, followed by stirring at room temperature for 3 hours.The reaction solution was concentrated under reduced pressure, and the residue was dissolved in dichloromethane (1.5 mL)Under ice cooling, a solution of zirconium (IV) chloride (0.264 g) and the compound obtained in Example 1a (0.200 g) in dichloromethane (2 mL) was added.After stirring the reaction mixture at room temperature for 2 hours, water was added and the mixture was extracted with ethyl acetate.The organic layer was washed with saturated saline and dried over anhydrous sodium sulfate.The organic layer was concentrated under reduced pressure, and the residue was purified by silica gel column chromatography(Ethyl acetate / hexane) to give the title compoundThe title compound (0.150 g) was obtained as a colorless amorphous solid.
 

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