Home Cart Sign in  
Chemical Structure| 1754-46-7 Chemical Structure| 1754-46-7

Structure of 1754-46-7

Chemical Structure| 1754-46-7

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1754-46-7 ]

CAS No. :1754-46-7
Formula : C11H17O3P
M.W : 228.22
SMILES Code : CC1=CC=C(P(OCC)(OCC)=O)C=C1
MDL No. :MFCD00015669

Safety of [ 1754-46-7 ]

Application In Synthesis of [ 1754-46-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1754-46-7 ]

[ 1754-46-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1754-46-7 ]
  • [ 3366-72-1 ]
YieldReaction ConditionsOperation in experiment
87% With hydrogenchloride; In water; for 17.5h;Reflux;Kinetics; Mechanism; General procedure: A mixture of phosphonate (3.8 mmol, 1a: 0.75 g, 1b: 0.80 g, 1c: 0.90 g,1d: 1.3 g, 1e: 0.90 g, 1f: 0.95 g), conc. HCl (1.0 ml, 12.0 mmol) and water(2.0 ml) was stirred at reflux for 45 min to 17.5 h. Evaporation of the organicphase in vacuo and recrystallization from methanol afforded a solid residuethat was analyzed by 31P NMR spectroscopy and LC-MS. To monitor thehydrolyses, aliquots were taken and simply evaporated. The 31P NMR andmass spectral data for phosphonates 1a-f, phosphonic monoesters 2a-f,and phosphonic acids 3a-c are summarized in Table S1 (see OnlineSupplementary Materials)
 

Historical Records