Alternatived Products of [ 179555-37-4 ]
Product Details of [ 179555-37-4 ]
CAS No. : | 179555-37-4 |
MDL No. : | |
Formula : |
C9H12N2O
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Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
164.20
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Pubchem ID : | - |
Synonyms : |
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Safety of [ 179555-37-4 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 179555-37-4 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 179555-37-4 ]
- 1
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[ 57963-11-8 ]
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[ 823-39-2 ]
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[ 179555-37-4 ]
Yield | Reaction Conditions | Operation in experiment |
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With acetic anhydride; In dichloromethane; |
Acetic anhydride (2.0 mL, 21 mmol) and 500 mg (4.09 mmol) of a 4:1 mixture of <strong>[823-39-2]2-amino-3,4-dimethylpyridine</strong> and 2-amino-4,5-dimethylpyridine (prepared by the method of W. O. Siegl, J. Heterocycl. Chem. 1981, 18, 1613-1618) were heated in a 135-140° C. oil bath for 2 h. The solution was concentrated on a rotary evaporator and the residue was chromatographed twice on silica gel, eluted with 30-50percent ethyl acetate in dichloromethane to give 71 mg of pure 2-acetamido-4,5-dimethylpyridine. 1 H NMR (200 MHz, CDCl3): delta 8.28 (bs, 1H), 8.00 (s, 1H), 7.97 (s, 1H), 2.29 (s, 3H), 2.19 (s, 3H), 2.17 (s, 3H). |