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Chemical Structure| 18303-03-2 Chemical Structure| 18303-03-2

Structure of 18303-03-2

Chemical Structure| 18303-03-2

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Product Details of [ 18303-03-2 ]

CAS No. :18303-03-2
Formula : C11H13NO4S
M.W : 255.29
SMILES Code : O=C(OCC=C)NS(=O)(C1=CC=C(C)C=C1)=O

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Application In Synthesis of [ 18303-03-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 18303-03-2 ]

[ 18303-03-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 14437-03-7 ]
  • [ 107-18-6 ]
  • [ 18303-03-2 ]
YieldReaction ConditionsOperation in experiment
74% at 100℃; for 0.5h;Sealed tube; Microwave irradiation; General procedure: The 4-substituted methyl (phenylsulfonyl)carbamate was dissolved in the chosen alcohol (2 mL) in a microwave vial, which was closed using an aluminum open-top seal with PTFE-faced septum. The reaction mixture was heated under microwave irradiation at 100-120 oC for 20-60 min. The crude reaction mixture was concentrated under reduced pressure and the residue was purified using silica gel column chromatography to yield the desired (aryl)carbamate.
 

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