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Chemical Structure| 18370-81-5 Chemical Structure| 18370-81-5

Structure of 18370-81-5

Chemical Structure| 18370-81-5

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Product Details of [ 18370-81-5 ]

CAS No. :18370-81-5
Formula : C3H8BrN
M.W : 138.01
SMILES Code : NCCCBr
MDL No. :MFCD00044486

Safety of [ 18370-81-5 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H301-H311-H331-H341
Precautionary Statements:P201-P202-P261-P264-P270-P271-P280-P302+P352-P304+P340-P308+P313-P310-P330-P361-P403+P233-P405-P501
Class:6.1
UN#:2810
Packing Group:

Application In Synthesis of [ 18370-81-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 18370-81-5 ]

[ 18370-81-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 18370-81-5 ]
  • [ 69506-85-0 ]
  • C15H28N6(2+)*2Br(1-) [ No CAS ]
YieldReaction ConditionsOperation in experiment
In ethanol; at 80℃; for 24h;Inert atmosphere; Step 2: 1,3-propyl imidazole and 0.01mol of 3-bromo-propylamine hydrobromide was added to a 0.02mol 40mL of anhydrous ethanol solvent, in the N2 after heating in an oil bath to protect the 80C, the reaction was refluxed for 24h, using the method for removing the solvent by rotary evaporation, the solvents and other volatile unreacted materials after the net, with a small amount of the reaction product was dissolved in water, and adding 4 to 7 of the solid KOH PH value of the solution was adjusted to 10 to reduce a protected amino group, the resulting solvent was distilled off under reduced pressure to remove the majority of the water and dried in vacuo to constant weight, the mass ratio of 4: 1 ethanol - tetrahydrofuran solution was extracted product after collecting the filtrate was evaporated under reduced pressure to recover the solvent again dried to constant weight in vacuo, a yellow viscous liquid available bis-(3-aminopropyl-1-imidazolyl)propylidene-dibromo salt.
 

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