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Chemical Structure| 184870-07-3 Chemical Structure| 184870-07-3

Structure of 184870-07-3

Chemical Structure| 184870-07-3

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Product Details of [ 184870-07-3 ]

CAS No. :184870-07-3
Formula : C17H13N5O2
M.W : 319.32
SMILES Code : O=C(C1=NC(C(NC2=CC=CN=C2)=O)=CC=C1)NC3=CC=CN=C3

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Application In Synthesis of [ 184870-07-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 184870-07-3 ]

[ 184870-07-3 ] Synthesis Path-Downstream   1~3

  • 1
  • nickel(II) chloride hexahydrate [ No CAS ]
  • [ 499-49-0 ]
  • [ 184870-07-3 ]
  • [Ni(N,N'-bis(pyridine-3-yl)pyridine-2,6-dicarboxamide)(5-methylisophthalicacid(-2H))(H2O)]*3H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
34% With sodium hydroxide; In water; at 120℃; for 96h;Autoclave; A mixture of NiCl26H2O (0.048 g, 0.2 mmol), L1 (0.032 g,0.1 mmol), H2mip (0.027 g, 0.15 mmol), water (8 mL), and NaOH(0.016 g, 0.3 mmol) was placed in a 25 mL Teflon reactor. Themixture was heated at 120 C for 4 d. Afterwards the autoclavewas gradually cooled to room temperature. Blue block-shapedcrystals of 1 were obtained in 34percent yield (based on Ni). IR (KBr,cm1): 3230 w, 1662 m, 1608 m, 1543 s, 1485 m, 1371 m, 1273 w.
  • 2
  • zinc(II) nitrate hexahydrate [ No CAS ]
  • [ 499-49-0 ]
  • [ 184870-07-3 ]
  • [Zn(N,N'-di(pyridin-3-yl)pyridine-2,6-dicarboxamide)(5-methylisophthalate)]H2O}n [ No CAS ]
YieldReaction ConditionsOperation in experiment
76% With sodium hydroxide; In water; at 120℃; for 96h;pH 6.7;Autoclave; N, N'-bis (3-pyridyl) pyridine-2,6-dicarboxamide was prepared by the procedure of Example 1,0.10 mmol of <strong>[499-49-0]5-methylisophthalic acid</strong> and 10 mL of H2O were successively added to a 25 mL beaker and stirred at room temperature40min, tooTo the suspension mixture, the pH of the suspension mixture was adjusted to 6.7 with 0.5 mol / L NaOH solution, transferred to 25 mL ofHigh pressure antiShould be in the kettle, to 5 ° C / h heating rate to 120 ° C heating, heat and water under the conditions of 96h to 2.5 ° C / h of the cooling rateRate will be warmDegrees to room temperature, to be colorless crystal block, with deionized water and ethanol alternately washed 4 times, at room temperature to dry naturally,Get [etaetaAlpha0 (pirho)] · H20} n, the yield of 76percent,
  • 3
  • cadmium(II) chloride hexahydrate [ No CAS ]
  • [ 499-49-0 ]
  • [ 184870-07-3 ]
  • [Cd2(N,N'-di(pyridin-3-yl)pyridine-2,6-dicarboxamide)(5-methylisophthalate)2](H2O)2H2O}n [ No CAS ]
 

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