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CAS No. : | 1894191-97-9 | MDL No. : | N/A |
Formula : | C26H26NO2P | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | MLHMEHOYQRTGQZ-UHFFFAOYSA-N |
M.W : | 415.46 | Pubchem ID : | 11177490 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P280-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
74% | With triethylamine In tetrahydrofuran; toluene at 0 - 20℃; | |
1.88 g | With triethylamine In toluene at 0℃; for 1h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: PCl3 / 6 h / Heating 2: 1.88 g / triethylamine / toluene / 1 h / 0 °C | ||
Multi-step reaction with 2 steps 1: PCl3 / 8 h / Heating 2: 74 percent / triethylamine / toluene; tetrahydrofuran / 0 - 20 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Stage #1: di-n-propylamine With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.5h; Inert atmosphere; Stage #2: With phosphorus trichloride In tetrahydrofuran; hexane at 0 - 20℃; for 1.16667h; Inert atmosphere; Stage #3: (S)-[1,1']-binaphthalenyl-2,2'-diol With triethylamine In tetrahydrofuran; hexane at 0 - 20℃; Inert atmosphere; |
A287873[ N/A ]
N,N-Dipropyldinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-amine
Reason: Racemic-enantiomer
A1270639[ 802902-36-9 ]
(11bS)-N,N-Dipropyldinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-amine
Reason: Optical isomers