Alternatived Products of [ 1895077-69-6 ]
Product Details of [ 1895077-69-6 ]
CAS No. : | 1895077-69-6 |
MDL No. : | MFCD34165593 |
Formula : |
C26H16O8
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | YPGWWACOIFPAKG-UHFFFAOYSA-N |
M.W : |
456.40
|
Pubchem ID : | 139035988 |
Synonyms : |
|
Safety of [ 1895077-69-6 ]
Application In Synthesis of [ 1895077-69-6 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 1895077-69-6 ]
- 1
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[ 1895077-74-3 ]
-
[ 1895077-69-6 ]
Yield | Reaction Conditions | Operation in experiment |
87% |
Stage #1: tetramethyl 5,5'-(naphthalene-1,5-diyl)diisophthalate With lithium hydroxide monohydrate In tetrahydrofuran; methanol; water at 69.84℃; for 24h; Inert atmosphere;
Stage #2: With hydrogenchloride In methanol |
|
52% |
With sodium hydroxide In tetrahydrofuran; methanol Reflux; |
|
Reference:
[1]Zhang, Mingxing; Zhou, Wei; Pham, Tony; Forrest, Katherine A.; Liu, Wenlong; He, Yabing; Wu, Hui; Yildirim, Taner; Chen, Banglin; Space, Brian; Pan, Yi; Zaworotko, Michael J.; Bai, Junfeng
[Angewandte Chemie - International Edition, 2017, vol. 56, # 38, p. 11426 - 11430][Angew. Chem., 2017, vol. 129, # 38, p. 11584 - 11588]
[2]Chen, Fengli; Bai, Dongjie; Jiang, Donghao; Wang, Yao; He, Yabing
[Dalton Transactions, 2017, vol. 46, # 34, p. 11469 - 11478]