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[ CAS No. 19227-14-6 ]

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Chemical Structure| 19227-14-6
Chemical Structure| 19227-14-6
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Product Details of [ 19227-14-6 ]

CAS No. :19227-14-6 MDL No. :MFCD00019951
Formula : C7H7BrN2O Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W :215.05 g/mol Pubchem ID :-
Synonyms :

Safety of [ 19227-14-6 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P362-P403+P233-P501 UN#:
Hazard Statements:H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 19227-14-6 ]

  • Upstream synthesis route of [ 19227-14-6 ]
  • Downstream synthetic route of [ 19227-14-6 ]

[ 19227-14-6 ] Synthesis Path-Upstream   1~2

  • 1
  • [ 19227-14-6 ]
  • [ 22265-36-7 ]
YieldReaction ConditionsOperation in experiment
68% for 96 h; Reflux; Inert atmosphere General procedure: Compound 44b (150 mg, 1.0 mmol) was boiled under reflux withHCOONH4 (403 mg, 6.3 mmol) and Pd/C (10percent, 150 mg) in AcOH (5 mL) for4 d under Ar. The cooled mixture was filtered (Celite®). Aq. NaOH(1.0 M, 20 mL) was added to the evaporation residue and the mixture wasextracted (EtOAc, 3 ). Drying andevaporation gave 44b (82 mg, 61percent) as a white powder.
Reference: [1] Bioorganic and Medicinal Chemistry, 2015, vol. 23, # 13, p. 3013 - 3032
[2] ChemMedChem, 2015, vol. 10, # 2, p. 360 - 367
  • 2
  • [ 19227-14-6 ]
  • [ 55368-42-8 ]
Reference: [1] Synthetic Communications, 2011, vol. 41, # 15, p. 2195 - 2199
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