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Chemical Structure| 19340-88-6 Chemical Structure| 19340-88-6

Structure of 19340-88-6

Chemical Structure| 19340-88-6

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Product Details of [ 19340-88-6 ]

CAS No. :19340-88-6
Formula : C11H15NO2
M.W : 193.24
SMILES Code : O=C(NCC1=CC=CC=C1)CCCO

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Application In Synthesis of [ 19340-88-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 19340-88-6 ]

[ 19340-88-6 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 2142-06-5 ]
  • [ 19340-88-6 ]
YieldReaction ConditionsOperation in experiment
99% With bis(1,5-cyclooctadiene)diiridium(I) dichloride; hydrogen; sodium t-butanolate; In isopropyl alcohol; at 40℃; under 30003.0 Torr; for 12h;Autoclave; Sealed tube; Add 38 mg of <strong>[2142-06-5]1-benzylpyrroline-2,5-dione</strong> (0.2 mmol), 2.2 mg of sodium tert-butoxide, and 2 ml of isopropanol under nitrogen protection. Add 5 mul of 0.001 M catalyst (S / C = 40,000), then the reaction flask was transferred to an autoclave, the reaction kettle was tightened, 4 MPa of hydrogen was charged, and the reaction was carried out at 40 C for 12 hours. After the reaction was completed, the mixture was naturally cooled to room temperature, and the hydrogen was carefully released. The celite was filtered, and the organic solvent was removed from the filtrate to obtain 38 mg of a yellow oil with a yield of 99%.
 

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