Home Cart Sign in  
Chemical Structure| 19500-05-1 Chemical Structure| 19500-05-1

Structure of 19500-05-1

Chemical Structure| 19500-05-1

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 19500-05-1 ]

CAS No. :19500-05-1
Formula : C10H11NO
M.W : 161.20
SMILES Code : CC1=C(OC)C=CC2=C1NC=C2
MDL No. :MFCD09027025

Safety of [ 19500-05-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H317
Precautionary Statements:P280

Application In Synthesis of [ 19500-05-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 19500-05-1 ]

[ 19500-05-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 4837-88-1 ]
  • [ 1826-67-1 ]
  • [ 19500-05-1 ]
YieldReaction ConditionsOperation in experiment
27% In tetrahydrofuran; at -40℃; for 0.5h; 6-Methoxy-7-methyl- 1 H-indolc:To a solution of l-methoxy-2-methyl~3~nitro-benzene (5.00 g, 29.9 mmol) in THF ( 100 mL) was added vinyl magnesium bromide (89.9 mL, 89.9 mmol) in one portion at -40 C. The mixture was stirred at -40 C for 30 min, was quenched by pouring into aqueous ammonium chloride saturated solution. The aqueous solution was extracted with EtOAc. The combined organic phases were dried over MgSO4 and concentrated in vacuo. The crude oil was purified by column chromatography (hexanes to 20% EtOAc in hexanes gradient) to give 6-methoxy- 7-methyl- l H-indoie (1.32 g, 27%) as brown solid. 1H NMR (400 MHz, CDCh) ?: 7.94 (br, IH), 7.46 (m, IH), 7.16 (m, IH), 6.89 (m, IH), 6.54 (m, IH), 3.94 (s, 3H), 2.40 (s, 3H); ESMS mA- 162 (M+H)+
 

Historical Records

Technical Information

Categories