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Chemical Structure| 19535-47-8 Chemical Structure| 19535-47-8

Structure of 19535-47-8

Chemical Structure| 19535-47-8

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Product Details of [ 19535-47-8 ]

CAS No. :19535-47-8
Formula : C18H10N4
M.W : 282.30
SMILES Code : C12=CC=CN=C1C3=NC=CC=C3C4=NC5=CC=CC=C5N=C42
MDL No. :MFCD28125537
InChI Key :BVQAWSJMUYMNQN-UHFFFAOYSA-N
Pubchem ID :3081616

Safety of [ 19535-47-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 19535-47-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 19535-47-8 ]

[ 19535-47-8 ] Synthesis Path-Downstream   1~2

  • 1
  • oxovanadium(IV) sulfate [ No CAS ]
  • [ 19535-47-8 ]
  • [ 1119-34-2 ]
  • [ 90-02-8 ]
  • [VO(N-salicylidene-L-arginine(-1H))(dipyrido[3,2-a:2',3'-c]phenazine)]Cl [ No CAS ]
  • 2
  • [ 19535-47-8 ]
  • copper(II) perchlorate hexahydrate [ No CAS ]
  • [ 414864-00-9 ]
  • ClO4(1-)*C33H23CuN6O4S(1+) [ No CAS ]
YieldReaction ConditionsOperation in experiment
79.8% With potassium hydroxide; In methanol; water; at 25℃; for 0.5h; Copper(ll) perchlorate hexahydrate (0.1090g; 0.294 mmol; 1 eq; limiting reagent) was dissolved in the minimum volume (1 ml) of Dl H2O. Hot methanolic solutions of Belinostat (0.0934g; 0.294 mmol; 1 eq; 4ml) and DPPZ (0.0828g; 0.294 mmol; 1 eq; 1 ml) were added sequentially and the resulting suspension was left to stir at room temperature for 30 minutes. A solid precipitate was filtered and dried under vacuum. [Cu(Belinostat-iH)(DPPZ)]CIC>4, green solid, 178.8 mg, 79.8 %. [Cu(Belinostat-1H)(DPPZ)]ClO4 ? MeOH requires C - 51.39%; H - 3.42%; N - 10.58%; Cu - 8.00%; CI - 4.46%. Found C - 51.35%; H - 2.96%; N - 10.75%; Cu - 7.93%; CI - 4.70%. ESI-MS ([M-H]+; MeOH) 661 .9 ([Cu(Belionstat IH)(DPPZ)]+) 345 ([Cu(DPPZ)]+). ATR-IR (cm-1) 1510, 1019 & 1 130.
 

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[ 19535-47-8 ]

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