Home Cart Sign in  
Chemical Structure| 197313-74-9 Chemical Structure| 197313-74-9

Structure of 197313-74-9

Chemical Structure| 197313-74-9

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 197313-74-9 ]

CAS No. :197313-74-9
Formula : C21H15NO2
M.W : 313.35
SMILES Code : O=C(C1=CC=CC2=C1NC(C3=CC=CC=C3)=C2C4=CC=CC=C4)O
MDL No. :MFCD00572872

Safety of [ 197313-74-9 ]

Application In Synthesis of [ 197313-74-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 197313-74-9 ]

[ 197313-74-9 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 119-53-9 ]
  • [ 118-92-3 ]
  • anthranilic acid-hydrochloride [ No CAS ]
  • [ 3469-20-3 ]
  • [ 197313-74-9 ]
  • 2
  • [ 451-40-1 ]
  • [ 33906-30-8 ]
  • [ 197313-74-9 ]
YieldReaction ConditionsOperation in experiment
24% <strong>[33906-30-8]2-hydrazinobenzoic acid hydrochloride</strong> (5.00 g, 30.08 mmol) and deoxybenzoin (5.90 g, 30.08 mmol) was refluxed in ACOH (100 ml) for 30 min, cone. HCI (50 ml) was added and mixture refluxed for 4 h. Water (800 ml) was added and a white solid precipitated. The solid was filtered, washed with water and recryst. from EtOAc (100 ml). Yield 2.23 g (24%); white solid. Mp. 262 C. 'H NMR (400 MHz, DMSO-d6) 6 7. 18 (t, J=8 Hz, 1 H), 7.27-7. 47 (M, 10 H), 7.75 (d, J=8 Hz, 1 H), 7.82 (d, J=8 Hz, 1 H), 10.73 (s, 1 H), 13.19 (s, 1 H). 13C NMR (100 MHz, DMSO-d6) 8 113. 80,113. 99,119. 68,124. 08,124. 72,126. 47,127. 97,128. 48,128. 72, 129.36, 129.86, 131.69, 134.35, 135.05, 135.38, 167.94. Found: 313.1117 (M). Calc. for C2LHL5NO2 : 313.1103. CAS [197313-74-9].
 

Historical Records

Technical Information

Categories