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Chemical Structure| 19930-62-2 Chemical Structure| 19930-62-2

Structure of 19930-62-2

Chemical Structure| 19930-62-2

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Product Details of [ 19930-62-2 ]

CAS No. :19930-62-2
Formula : C12H10Br2
M.W : 314.02
SMILES Code : CC1=C(C)C(Br)=C2C=CC=CC2=C1Br
MDL No. :MFCD01652201

Safety of [ 19930-62-2 ]

Application In Synthesis of [ 19930-62-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 19930-62-2 ]

[ 19930-62-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 952514-79-3 ]
  • [ 19930-62-2 ]
  • C50H36N4 [ No CAS ]
YieldReaction ConditionsOperation in experiment
58.19% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In ethanol; water; toluene; at 80℃; for 16h; 1,4-Dibromo-2,3-dimethylnaphthalene (10.0 g,31.85 mmol) was reacted with 4- (l-phenyl-lH-benzo [ d]imidazol-2-yl) phenylboronic acid (22.01 g, 70.06 mmol) was placed in a reaction flask followed by toluene 150ml. K2CO3(22.01 g, 159.23 mmol) was dissolved in 90 ml deionized water and added to the reaction flask. To the reaction flask was added Pd(PPh3)4(3.68 g, 3.18 mmol) And refluxed at 80 C for 16 hours.After the reaction,200 ml of deionized water was added and the mixture was stirred to room temperature. The solid was filtered off and washed with deionized water and toluene. The solid was furtherstirred for 30 minutes byadding 200ml of deionized water, 50 ml of methanol and 150 ml of toluene , Then filtered, repeated 2 times.Ovendry the solid to obtain a white solid compound A3 (12.84g, 58.19% yield).
 

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