Home Cart Sign in  
Chemical Structure| 33421-40-8 Chemical Structure| 33421-40-8
Chemical Structure| 33421-40-8

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of 2-Amino-5-phenylpyridine

CAS No. :33421-40-8
Formula : C11H10N2
M.W : 170.21
SMILES Code : NC1=NC=C(C2=CC=CC=C2)C=C1
MDL No. :MFCD01692452
InChI Key :OAPVIBHQRYFYSE-UHFFFAOYSA-N
Pubchem ID :105097

Safety of 2-Amino-5-phenylpyridine

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of 2-Amino-5-phenylpyridine

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 33421-40-8 ]

[ 33421-40-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 33421-40-8 ]
  • [ 1798-06-7 ]
  • [ 1243245-74-0 ]
YieldReaction ConditionsOperation in experiment
With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20℃; for 2h; To a solution of 2-<strong>[1798-06-7](4-iodophenyl)acetic acid</strong> 53-1 (816 mg, 3.14 mmol), 5- phenylpyridin-2-amine 53-2 (534mg, 3.14 mmol) and HATU (1.19 g, 3.14 mmol) in DMF (1 mL) was added DIEA (1.57 mL, 9.42 mmol) at room temperature. The mixture was stirred at room temperature for 2 hours. The mixture was diluted with ethyl acetate (50 mL), washed with saturated NaHCO3 aqueous solution, water and brine, dried over Na2SO4, and concentrated by rotary evaporation. The crude product was purified by silica gel flash chromatography, eluted with 40% ethyl acetate in hexane to give 2-(4-Iodophenyl)-N-(5-phenylpyridin-2-yl)acetamide 53-3 as pale yellow solid. MS m/z 415.2 (M + 1)
 

Historical Records

Technical Information

Categories