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Chemical Structure| 20057-77-6 Chemical Structure| 20057-77-6

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Chemical Structure| 20057-77-6

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Product Details of [ 20057-77-6 ]

CAS No. :20057-77-6
Formula : C14H14S4
M.W : 310.52
SMILES Code : CSC1=CC=C(SSC2=CC=C(SC)C=C2)C=C1
MDL No. :N/A

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Application In Synthesis of [ 20057-77-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 20057-77-6 ]

[ 20057-77-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 16001-93-7 ]
  • [ 20057-77-6 ]
  • [ 151425-93-3 ]
YieldReaction ConditionsOperation in experiment
25% EXAMPLE 4 tetramethyl (4-methylthiophenyl)thiomethanediphosphonate STR14 3.87 g of the target compound was obtained in the form of a pale yellow oily substance by reacting 9.28 g (40 mmol) of <strong>[16001-93-7]tetramethyl methylenediphosphonate</strong> with 12.42 g (40 mmol) of bis(4-methylthiophenyl)disulfide, according to the same method as Example 1-(b). Yield: 25% 1 H-NMR (CDCl3) [ppm]: delta2.47 (s,3H), 3.36 (t,J=22 Hz,1H), 3.75-4.00 (m, 12H), 7.09-7.30 (m, 2H), 7.44-7.65 (m, 2H) IR (KBr) [cm- ]: 2960, 2858, 1576, 1479, 1446, 1392, 1259, 1185, 1106, 1029, 853 MASS (FAB) m/z: 387 (M+H)+ Elementary Analysis (as C12 H20 O6 P2 S2) Calculated values (%): C 37.31 H 5.23 Observed values (%): C 37.33 H 5.30
 

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