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[ CAS No. 204078-26-2 ] {[proInfo.proName]}

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Chemical Structure| 204078-26-2
Chemical Structure| 204078-26-2
Structure of 204078-26-2 * Storage: {[proInfo.prStorage]}
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Product Details of [ 204078-26-2 ]

CAS No. :204078-26-2 MDL No. :MFCD11145772
Formula : C10H12N2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 160.22 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 204078-26-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 204078-26-2 ]

[ 204078-26-2 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 204078-26-2 ]
  • [ 1027241-69-5 ]
  • 2-[N-(3-cyanophenyl)-N-isopropylcarbamoyl]-4-ethylthio-5-methyl-4-isoxazolin-3-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
With triethylamine In toluene at 20℃; for 0.583333h;
  • 2
  • [ 75-30-9 ]
  • [ 873-74-5 ]
  • [ 204078-26-2 ]
YieldReaction ConditionsOperation in experiment
With sodium carbonate In methanol Heating;
  • 3
  • [ 204078-26-2 ]
  • [ 74-88-4 ]
  • 4-(N-isopropyl-N-methylamino)benzonitrile [ No CAS ]
YieldReaction ConditionsOperation in experiment
In methanol Heating;
  • 4
  • [ 1194-02-1 ]
  • [ 75-31-0 ]
  • [ 204078-26-2 ]
YieldReaction ConditionsOperation in experiment
30% With potassium carbonate In dimethyl sulfoxide at 100℃; for 16h; 146.1 A solution mixture of 4-fluorobenzonitrilre (3.0 g, 24.79 mmol), isopropylamine (10 mL,122.l4mmol) and K2003 (3.41 g, 24.72 mmol) in DMSO (10 mL) was stirred at 100 CC for16 h. The reaction mixture was partitioned between water (50 mL) and ethyl acetate (2 x50 mL). The ethyl acetate layer was washed with brine (100 mL), dried over anhydrousNa2SO4 and concentrated to afford 1 .2 g (30 %) of 4-(isopropylamino)benzonitrlle 146-1as a white solid. 1H NMR (400 MHz, DMSO-d6): 7.42 (d, J= 8.8 Hz, 2H), 6.60 (d, J=8.8 Hz, 2H), 6.53 (d, J= 7.4 Hz, 1H), 3.56-3.64 (m, 1H), 1.13 (d, J= 6.6 Hz, 6H).
R.4 4-Isopropylaminobenzonitrile REFERENCE EXAMPLE 4 4-Isopropylaminobenzonitrile By using the same method as described in Reference Example 3, the subject compound is synthesised from 4-fluorobenzonitrile and isopropylamine. 1H-NMR (CDCl3) δ (ppm): 1.23 (6H, d, J=6.6 Hz), 3.61-3.69 (1H, m), 4.22 (1H, br), 6.53 (2H, d, J=8.9 Hz), 7.38 (2H, d, J=8.9 Hz).
R.4 4-Isopropylaminobenzonitrile REFERENCE EXAMPLE 4 4-Isopropylaminobenzonitrile According to a similar manner to that in Reference Example 3, the title compound was synthesised from 4-fluorobenzonitrile and isopropylamine. 1 H-NMR (CDCl3) δ (ppm): 1.23(6H, d, J=6.6 Hz), 3.61-3.69(1H, m), 4.22(1H, br), 6.53(2H, d, J=8.9 Hz), 7.38(2H, d, J=8.9 Hz).
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