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Chemical Structure| 20921-96-4 Chemical Structure| 20921-96-4

Structure of 20921-96-4

Chemical Structure| 20921-96-4

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Product Details of [ 20921-96-4 ]

CAS No. :20921-96-4
Formula : C10H9NO2
M.W : 175.18
SMILES Code : O=C(OC)CC1=CC=CC=C1C#N
MDL No. :MFCD02181139
InChI Key :MBLNSABLVSWAKD-UHFFFAOYSA-N
Pubchem ID :1512623

Safety of [ 20921-96-4 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302
Precautionary Statements:P280-P305+P351+P338

Application In Synthesis of [ 20921-96-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 20921-96-4 ]

[ 20921-96-4 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 186581-53-3 ]
  • [ 18698-99-2 ]
  • [ 20921-96-4 ]
  • 2
  • [ 18698-99-2 ]
  • [ 18107-18-1 ]
  • [ 20921-96-4 ]
YieldReaction ConditionsOperation in experiment
95% In tetrahydrofuran; methanol; at 15 - 30℃; for 2h; Compound 10.1 (5 g, 31 mmol) And (trimethylsilane) diazomethane (3.5 g, 31 mmol) Tetrahydrofuran (20mL) The mixed solution with methanol (20 mL) was stirred at room temperature for 2 hours. Then the reaction system is directly concentrated, The residue was chromatographed on silica gel (30percent ethyl acetate petroleum ether) Purification afforded compound 10.2 (5.1 g, yield: 95percent) as a colourless oil.
 

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