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CAS No. : | 2099033-14-2 | MDL No. : | N/A |
Formula : | C48H37O4P | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 708.78 | Pubchem ID : | - |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P301+P312-P302+P352-P304+P340-P305+P351+P338 | UN#: | |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
94% | Stage #1: (R)-3,3'-di(anthracen-9-yl)-5,5',6,6',7,7',8,8'-octahydro-[1,1'-binaphthalene]-2,2'-diol With pyridine; trichlorophosphate at 80℃; for 2h; Stage #2: With water at 40℃; for 0.166667h; Stage #3: With hydrogenchloride at 100℃; for 0.0833333h; Further stages.; | |
63% | With pyridine; trichlorophosphate at 80℃; for 2.5h; Inert atmosphere; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
97% | Stage #1: C8H12O3; 4-methoxy-aniline In tetrahydrofuran at -50℃; for 0.333333h; Stage #2: (R)-3,3'-di(anthracen-9-yl)-5,5',6,6',7,7',8,8'-octahydro-[1,1'-binaphthalene]-2,2'-diyl hydrogen phosphate In tetrahydrofuran at -50℃; for 0.216667h; Stage #3: C15H36O2Si4 In tetrahydrofuran at -50℃; for 13h; enantioselective reaction; |
A795910[ 1011465-29-4 ]
(R)-3,3'-Bis(9-anthracenyl)-5,5',6,6',7,7',8,8'-octahydro-1,1'-bi-2-naphthyl HydrogenPhosphate
Reason: Optical isomers