Home Cart Sign in  
Chemical Structure| 212204-36-9 Chemical Structure| 212204-36-9

Structure of 212204-36-9

Chemical Structure| 212204-36-9

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 212204-36-9 ]

CAS No. :212204-36-9
Formula : C13H16ClNO4S
M.W : 317.79
SMILES Code : O=C(N1[C@H](CS(=O)(Cl)=O)CCC1)OCC2=CC=CC=C2
MDL No. :MFCD13190148

Safety of [ 212204-36-9 ]

Application In Synthesis of [ 212204-36-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 212204-36-9 ]

[ 212204-36-9 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 6216-63-3 ]
  • [ 212204-36-9 ]
  • 2
  • [ 4089-07-0 ]
  • [ 212204-36-9 ]
  • [ 1454845-43-2 ]
YieldReaction ConditionsOperation in experiment
With triethylamine; In dichloromethane; at 35℃;Cooling with ice; General procedure: NCS (534 mg, 4 mmol) was dissolved in a mixture of 2 M HCl (0.8 mL) and MeCN (4 mL). The resulting solution was cooled to 10 °C. A solution of thiolacetate 7 (1 mmol) in MeCN (1 mL) was added dropwise to the cooled solution at below 20 °C. The resulting solution was stirred at the same temperature for 30 min, and then diluted with isopropyl ether (5 mL). The organic layer was washed with aq NaCl (12percent, 3*5 mL) and then dried over anhydrous Na2SO4. After concentration in vacuo, the crude sulfonyl chloride 8 was obtained as colorless solids or pale yellow oil, and used directly without further purification.
 

Historical Records