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Chemical Structure| 2142-03-2 Chemical Structure| 2142-03-2

Structure of 2142-03-2

Chemical Structure| 2142-03-2

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Product Details of [ 2142-03-2 ]

CAS No. :2142-03-2
Formula : C15H11NO2
M.W : 237.25
SMILES Code : O=C1N(C2=CC=C(C)C=C2)C(C3=C1C=CC=C3)=O

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Application In Synthesis of [ 2142-03-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 2142-03-2 ]

[ 2142-03-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 59046-72-9 ]
  • [ 106-49-0 ]
  • [ 2142-03-2 ]
YieldReaction ConditionsOperation in experiment
86% With oxygen; copper(ll) bromide; In toluene; at 100℃; under 760.051 Torr; for 6h; A 50 mL round bottom flask was used as the reactor,0.2 mmol of o-phenynylbenzaldehyde represented by 1a was added,1.5 equivalents (0.3 mmol) of p-methylaniline of formula 2a and 10 mol% of CuBr2 as a catalyst,Then, 2 mL of toluene was added as the reaction solvent,The reaction atmosphere was O2 atmosphere (1 atm)And then placed in the adjustment of the temperature of 100 equipped with magnetic stirrer in the oil bath stirring,After 6 hours of reaction,By TLC detection until the reaction is complete.The reaction mixture was then filtered,Concentrated under reduced pressure,Column chromatography separation,To give the title compound of formula I-1 in 86% yield.
 

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