Alternatived Products of [ 21576-27-2 ]
Product Details of [ 21576-27-2 ]
CAS No. : | 21576-27-2 |
MDL No. : | MFCD11106791 |
Formula : |
C9H15NO3
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
185.22
|
Pubchem ID : | - |
Synonyms : |
|
Application In Synthesis of [ 21576-27-2 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 21576-27-2 ]
Yield | Reaction Conditions | Operation in experiment |
|
2-Ethoxy-3-carbethoxy-3,4,5,6-tetrahydro-pyridin, Dimethylsulfat; |
|
|
entspr. 1-Methyl-3-cyan-Verb., 4percentig. HCl, sd. A. (15h); |
|
|
die Verbdg. entsteht gleicherweise aus 3-(Aminoethoxymethylen)-Verbdg. (S.1978); |
|
|
1-Methyl-2-ethoxy-3-ethoxycarbonyl-3,4,5,6-tetrahydropyridin-methylsulfat (IV) (Dest./5mm); |
|
|
N-Methyl-piperidon-(2), Oxalsaeure-diethylester, K., Ae., etw. A. (neben N-Methyl-3-ethoxalyl-piperidon-(2)); |
|
|
N-Methyl-3-ethoxalyl-piperidon-(2) (Δ); |
|
|
N-Methyl-3-cyan-piperidon-(2), (Hydrolyse, Veresterung); |
|
- 2
-
[ 931-20-4 ]
-
[ 105-58-8 ]
-
[ 21576-27-2 ]
Yield | Reaction Conditions | Operation in experiment |
42% |
With sodium hydride In tetrahydrofuran for 7h; Heating; |
|
- 3
-
[ 21576-27-2 ]
-
[ 944276-44-2 ]
Yield | Reaction Conditions | Operation in experiment |
90% |
With sodium tetrahydroborate; calcium chloride In methanol at 20℃; for 14h; |
|
- 4
-
[ 21576-27-2 ]
-
ethyl 5-methyl-4-oxo-1,5-diazaspiro[2.5]octane-1-carboxylate
[ No CAS ]
Yield | Reaction Conditions | Operation in experiment |
|
Multi-step reaction with 3 steps
1: 90 percent / NaBH4; CaCl2 / methanol / 14 h / 20 °C
2: 59 percent / N,N-dicyclohexylcarbodiimide; CuI / toluene / 1.17 h / Heating
3: 46 percent / CaO / CH2Cl2 / 4 h / cooling |
|
- 5
-
[ 21576-27-2 ]
-
[ 1690-73-9 ]
Yield | Reaction Conditions | Operation in experiment |
|
Multi-step reaction with 2 steps
1: 90 percent / NaBH4; CaCl2 / methanol / 14 h / 20 °C
2: 59 percent / N,N-dicyclohexylcarbodiimide; CuI / toluene / 1.17 h / Heating |
|