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Chemistry
Organic Building Blocks
Benzene Compounds
2-(2-Formylphenoxy)-N-methylacetamide
Chemistry
Organic Building Blocks
Benzene Compounds
Benzene Compounds

[ CAS No. 216082-34-7 ]

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3d Animation Molecule Structure of 216082-34-7
Chemical Structure| 216082-34-7
Chemical Structure| 216082-34-7
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Product Details of [ 216082-34-7 ]

CAS No. :216082-34-7 MDL No. :MFCD11149391
Formula : C10H11NO3 Boiling Point : -
Linear Structure Formula :- InChI Key :N/A
M.W :193.20 g/mol Pubchem ID :-
Synonyms :

Safety of [ 216082-34-7 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 216082-34-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 216082-34-7 ]

[ 216082-34-7 ] Synthesis Path-Downstream   1~7

  • 1
  • [ 216082-34-7 ]
  • 2-methylcarbamoylmethoxy-benzoic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
66% With sodium chlorite; recorcinol In water; <i>tert</i>-butyl alcohol at 30 - 40℃; for 3h;
Reference： [1]Kwiecien [Polish Journal of Chemistry, 1998, vol. 72, # 10, p. 2254 - 2260]
  • 2
  • <i>N</i>-methyl-2-(2-methyliminomethyl-phenoxy)-acetamide [ No CAS ]
  • [ 216082-34-7 ]
YieldReaction ConditionsOperation in experiment
75% With hydrogenchloride
Reference： [1]Kwiecien [Polish Journal of Chemistry, 1998, vol. 72, # 10, p. 2254 - 2260]
  • 3
  • [ 89-95-2 ]
  • [ 216082-34-7 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: 60 percent / K2CO3 / dimethylformamide / 2 h / 92 - 96 °C 2: ethanol / 120 h / 20 °C 3: 75 percent / aq. HCl
Reference： [1]Kwiecien [Polish Journal of Chemistry, 1998, vol. 72, # 10, p. 2254 - 2260]
  • 4
  • [ 41873-61-4 ]
  • [ 216082-34-7 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: ethanol / 120 h / 20 °C 2: 75 percent / aq. HCl
Reference： [1]Kwiecien [Polish Journal of Chemistry, 1998, vol. 72, # 10, p. 2254 - 2260]
  • 5
  • [ 75270-15-4 ]
  • [ 74-89-5 ]
  • [ 216082-34-7 ]
YieldReaction ConditionsOperation in experiment
In tetrahydrofuran; dichloromethane at 20℃; for 16h; 6 (2-Formyl-phenoxy)-acetic acid (0.5 mmol) is dissolved in 1 mL of CH2Cl2. Oxalyl chloride (0.066 mL) is added along with one drop of DMF. After 1 hour, the solvent is removed from the mixture. The resultant residue is dissolved in 1 mL of CH2Cl2 and added to 1 mL of NH2 Me in THF (2 M) at ambient temperature. After 16 hours of stirring, the solvent is removed and the mixture is purified by preparative TLC (10% MeOH/EtOAc) to yield the product 2-(2-formyl-phenoxy)-N-methyl-acetamide as an off white solid: LC/MS (ES+): 194.1 (M+1)+.
Reference： [1]Current Patent Assignee: IRM LLC - US2009/325981, 2009, A1 Location in patent: Page/Page column 10
  • 6
  • [ 50487-61-1 ]
  • [ 216082-34-7 ]
  • C17H16ClN3O2S [ No CAS ]
YieldReaction ConditionsOperation in experiment
In dichloromethane for 0.166667h; 6 The 2-(2-formyl-phenoxy)-N-methyl-acetamide (0.0311 mmol) is added to 4-chloro-thiobenzoic acid hydrazide (0.0342 mmol) in 0.1 mL of CH2Cl2. After 10 minutes, DIEA (0.05 mL) and 2,4,6-trifluoro-benzoyl chloride (0.0467 mmol) are added. The mixture is kept at room temperature overnight. After removal of solvent, the residue is purified by preparative HPLC (20-100% MeCN/H2O gradient) to give the product 2-{2-[5-(4-chloro-phenyl)-3-(2,4,6-trifluoro-benzoyl)-2,3-dihydro-[1,3,4]thiadiazol-2-yl]-phenoxy}-N-methyl-acetamide as an off white solid: LC/MS (ES+): 520.1 (M+1)+.
Reference： [1]Current Patent Assignee: IRM LLC - US2009/325981, 2009, A1 Location in patent: Page/Page column 10
  • 7
  • [ 54704-34-6 ]
  • [ 216082-34-7 ]
  • C19H30N2O2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
Stage #1: L-1-methyl-2-cyclohexylethylamine; 2-(2-formyl-phenoxy)-N-methyl-acetamide In methanol at 100℃; for 2h; Stage #2: With methanol; sodium tetrahydroborate at 60℃; for 6h; 7.B Step B Aldehyde 3 (0.55 mmol), amine 4 (0.5 mmol) were dissolved in 0.6 ml MeOH, heated at 100° C for 2 hours, then mixture was cooled, NaBH4 (0.5 mmol) was added and stirred for 4 hours. The mixture was heated for 2 hours at 60° C, 3 ml of methanol and 0.2 g of C-18 chromatographic phase were added, stirred for 2 hours, filtered, evaporated and optionally dissolved in 0.5 mL of DMSO. The residue was purified using HPLC. Yield: 24- 47%. (0743) [00304] 8.56 (s, 1H), (0744) 7.19 (t, J = 8.0 Hz, 2H), 6.93 - 6.84 (m, 2H), 4.51 (s, 2H), 3.78 (d, J = 12.0 Hz, 1H), 3.65 (d, J = 12.1 Hz, 1H), 2.71 (d, J = 5.8 Hz, 2H), 2.66 (d, J = 4.6 Hz, 3H), 2.54 (s, 1H), 1.67 (d, J = 15.3 Hz, 5H), 1.35 (s, 1H), 1.20 (dd, J = 22.0, 9.6 Hz, 2H), 1.05 (d, J = 6.2 Hz, 3H), 0.86 (d, J = 12.3 Hz, 2H).
Reference： [1]Current Patent Assignee: HARVARD UNIVERSITY - WO2019/140265, 2019, A1 Location in patent: Paragraph 00302-00304

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