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Chemical Structure| 2206-83-9 Chemical Structure| 2206-83-9

Structure of 2206-83-9

Chemical Structure| 2206-83-9

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Product Details of [ 2206-83-9 ]

CAS No. :2206-83-9
Formula : C10H10Cl4
M.W : 272.00
SMILES Code : ClCC1=C(CCl)C=C(CCl)C(CCl)=C1

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Application In Synthesis of [ 2206-83-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 2206-83-9 ]

[ 2206-83-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 120068-37-3 ]
  • [ 2206-83-9 ]
  • N-1,3,4,6-tetrakis(1-(2,6-dichloro-4-trifluoromethylphenyl)-3-cyano-4-trifluoromethylsulfinyl-1H-pyrazol-5ylamino)benzyl [ No CAS ]
YieldReaction ConditionsOperation in experiment
85.4% With potassium hydroxide; In N,N-dimethyl-formamide; at 20℃; for 3h;Sonication; Microwave irradiation; Heating; (150 W in fixed power) was added 50 mL of N, N-dimethylformamide, 10.0 g of 3-cyano-4-trifluoromethylsulfinyl-5-amino-1- (2,6-dichloro 4-trifluoromethylphenyl) -1H-pyrazole, 2g KOH, and then add 7.6g1,3,4,6-tetrachlorobenzyl, ultrasonic vibration at room temperature for 60min, open the spray switch after the shock, through the trachea The mist was sent to the top of the microwave reactor, and the microwave reactor was turned on. The power was adjusted to 300W to start the heating reaction. When the solvent in the ultrasonic atomizer was about to dry, the atomization was stopped and the microwave reactor was shut down.After completion of the reaction, the product was washed with water and dried by filtration to obtain 14.96 g of compound 10.Yield: 85.4%.
 

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