[ CAS No. 22146-59-4 ] {[proInfo.proName]}

Name: 22146-59-4|(2S)-2-Acetamido-3,3-dimethylbutanoic acid|95%
Brand: Ambeed
SKU: A1080104
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DV 2D 3D

3d Animation Molecule Structure of 22146-59-4

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Quality Control of [ 22146-59-4 ]

COA NMR CNMR HPLC LC-MS

Related Doc. of [ 22146-59-4 ]

SDS Specification

Alternatived Products of [ 22146-59-4 ]

Product Details of [ 22146-59-4 ]

CAS No. :	22146-59-4	MDL No. :	MFCD08275827
Formula :	C₈H₁₅NO₃	Boiling Point :	-
Linear Structure Formula :	-	InChI Key :	WPPXAQGLXQAVTE-ZCFIWIBFSA-N
M.W :	173.21	Pubchem ID :	11469346
Synonyms :

Calculated chemistry of [ 22146-59-4 ] Expand+

Physicochemical Properties

Num. heavy atoms :	12
Num. arom. heavy atoms :	0
Fraction Csp3 :	0.75
Num. rotatable bonds :	4
Num. H-bond acceptors :	3.0
Num. H-bond donors :	2.0
Molar Refractivity :	45.08
TPSA :	66.4 Å²

Pharmacokinetics

GI absorption :	High
BBB permeant :	No
P-gp substrate :	No
CYP1A2 inhibitor :	No
CYP2C19 inhibitor :	No
CYP2C9 inhibitor :	No
CYP2D6 inhibitor :	No
CYP3A4 inhibitor :	No
Log Kp (skin permeation) :	-6.72 cm/s

Lipophilicity

Log Po/w (iLOGP) :	1.24
Log Po/w (XLOGP3) :	0.9
Log Po/w (WLOGP) :	0.62
Log Po/w (MLOGP) :	0.53
Log Po/w (SILICOS-IT) :	0.21
Consensus Log Po/w :	0.7

Druglikeness

Lipinski :	0.0
Ghose :	None
Veber :	0.0
Egan :	0.0
Muegge :	1.0
Bioavailability Score :	0.85

Water Solubility

Log S (ESOL) :	-1.22
Solubility :	10.5 mg/ml ; 0.0607 mol/l
Class :	Very soluble
Log S (Ali) :	-1.88
Solubility :	2.29 mg/ml ; 0.0132 mol/l
Class :	Very soluble
Log S (SILICOS-IT) :	-0.9
Solubility :	22.0 mg/ml ; 0.127 mol/l
Class :	Soluble

Medicinal Chemistry

PAINS :	0.0 alert
Brenk :	0.0 alert
Leadlikeness :	1.0
Synthetic accessibility :	1.67

Safety of [ 22146-59-4 ]

Signal Word:	Warning	Class:	N/A
Precautionary Statements:	P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P332+P313-P337+P313-P362-P403+P233-P405-P501	UN#:	N/A
Hazard Statements:	H315-H319-H335	Packing Group:	N/A
GHS Pictogram:

Application In Synthesis of [ 22146-59-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Upstream synthesis route of [ 22146-59-4 ]
Downstream synthetic route of [ 22146-59-4 ]

[ 22146-59-4 ] Synthesis Path-Upstream 1~1

1
[ 22146-59-4 ]
[ 20859-02-3 ]

Reference： [1] Bulletin of the Chemical Society of Japan, 1968, vol. 41, p. 2178 - 2179

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Isomers

Technical Information

• Acyl Group Substitution • Amide Hydrolysis • Amide Hydrolysis • Amides Can Be Converted into Aldehydes • Amines Convert Acyl Chlorides into Amides • Chan-Lam Coupling Reaction • Complex Metal Hydride Reductions • Formation of an Amide from an Amine and a Carboxylic Acid • Formation of an Amide from an Amine and a Carboxylic Acid • Hofmann Rearrangement • Hydride Reductions • Lawesson's Reagent • Preparation of Amines • Reactions of Amines • Reduction of an Amide to an Amine • Reduction of an Amide to an Amine • Specialized Acylation Reagents-Carbodiimides and Related Reagents • Specialized Acylation Reagents-Ketenes

Historical Records

Related Functional Groups of
[ 22146-59-4 ]

Amides

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P220	Keep/Store away from clothing/combustible materials.
P221	Take any precaution to avoid mixing with combustibles
P222	Do not allow contact with air.
P223	Keep away from any possible contact with water, because of violent reaction and possible flash fire.
P230	Keep wetted
P231	Handle under inert gas.
P232	Protect from moisture.
P233	Keep container tightly closed.
P234	Keep only in original container.
P235	Keep cool
P240	Ground/bond container and receiving equipment.
P241	Use explosion-proof electrical/ventilating/lighting/equipment.
P242	Use only non-sparking tools.
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P244	Keep reduction valves free from grease and oil.
P250	Do not subject to grinding/shock/friction.
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P260	Do not breathe dust/fume/gas/mist/vapours/spray.
P261	Avoid breathing dust/fume/gas/mist/vapours/spray.
P262	Do not get in eyes, on skin, or on clothing.
P263	Avoid contact during pregnancy/while nursing.
P264	Wash hands thoroughly after handling.
P265	Wash skin thouroughly after handling.
P270	Do not eat, drink or smoke when using this product.
P271	Use only outdoors or in a well-ventilated area.
P272	Contaminated work clothing should not be allowed out of the workplace.
P273	Avoid release to the environment.
P280	Wear protective gloves/protective clothing/eye protection/face protection.
P281	Use personal protective equipment as required.
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P284	Wear respiratory protection.
P285	In case of inadequate ventilation wear respiratory protection.
P231 + P232	Handle under inert gas. Protect from moisture.
P235 + P410	Keep cool. Protect from sunlight.
Response
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P311	Call a POISON CENTER or doctor/physician.
P312	Call a POISON CENTER or doctor/physician if you feel unwell.
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P315	Get immediate medical advice/attention.
P320
P302 + P352	IF ON SKIN: wash with plenty of soap and water.
P321
P322
P330	Rinse mouth.
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P342	If experiencing respiratory symptoms:
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P373	DO NOT fight fire when fire reaches explosives.
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P376	Stop leak if safe to do so. Oxidising gases (section 2.4) 1
P377	Leaking gas fire: Do not extinguish, unless leak can be stopped safely.
P378
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P390	Absorb spillage to prevent material damage.
P391	Collect spillage. Hazardous to the aquatic environment
P301 + P310	IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.
P301 + P312	IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
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P304 + P312	IF INHALED: Call a POISON CENTER or doctor/physician if you feel unwell.
P304 + P340	IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
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P305 + P351 + P338	IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
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P332 + P313	IF SKIN irritation occurs: Get medical advice/attention.
P333 + P313	IF SKIN irritation or rash occurs: Get medical advice/attention.
P335 + P334	Brush off loose particles from skin. Immerse in cool water/wrap in wet bandages.
P337 + P313	IF eye irritation persists: Get medical advice/attention.
P342 + P311	IF experiencing respiratory symptoms: call a POISON CENTER or doctor/physician.
P370 + P376	In case of fire: Stop leak if safe to Do so.
P370 + P378	In case of fire:
P370 + P380	In case of fire: Evacuate area.
P370 + P380 + P375	In case of fire: Evacuate area. Fight fire remotely due to the risk of explosion.
P371 + P380 + P375	In case of major fire and large quantities: Evacuate area. Fight fire remotely due to the risk of explosion.
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P401
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P410 + P412	Protect from sunlight. Do not expose to temperatures exceeding 50 oC/122oF.
P411 + P235	Keep cool.
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P501	Dispose of contents/container to ...
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Yield	Reaction Conditions	Operation in experiment
	In acetic acid
	Multi-step reaction with 2 steps 1.1: thionyl chloride / toluene; dimethylformamide / 25 h / 20 °C 1.2: toluene; dimethylformamide / 5 h / 20 °C 2.1: Alcalase (R) / toluene; aq. phosphate buffer / 50 h / 35 °C / pH 8.0
	Multi-step reaction with 2 steps 1.1: thionyl chloride / toluene; dimethylformamide / 25 h / 20 °C 1.2: 89.8 percent / toluene; dimethylformamide / 5 h / 20 °C 2.1: Alcalase (R) / toluene; aq. phosphate buffer / 50 h / 35 °C / pH 8.0

Yield	Reaction Conditions	Operation in experiment
50%	With sodium hydroxide In 1,4-dioxane; water at 0 - 20℃;
46%	Stage #1: L-tert-Leucine With sodium hydroxide In water at 0℃; Stage #2: acetyl chloride In 1,4-dioxane; water at 20℃;

Yield	Reaction Conditions	Operation in experiment
77%	With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 5h; Inert atmosphere;	(2R,6S,13aS,14aR,16aS,Z)-6-((S)-2-Acetamido-3,3-dimethylbutanamido)-2-((7-methoxy-3- methylquinoxalin-2-yl)oxy)-N-((1-methylcyclopropyl)sulfonyl)-5,16-dioxo- 1,2,3,6,7,8,9,10,11,13a,14,15,16,16a-tetradecahydrocyclopropa[e]pyrrolo[1,2-a] [1,4]diazacyclopentadecine-14a(5H)-carboxamide (P4-P5-2). A mixture of amine salt 11 (0.31 g, 0.45 mmol) and N-Ac-Tle-OH (0.10 g, 0.58 mmol) in anhydrous DMF (8 mL) was treated with DIEA (0.60 mL, 3.50 mmol) and HATU (0.35 g, 0.92 mmol). The resulting reaction mixture was stirred at room temperature for 5 h, then diluted with EtOAc (100 mL), and washed successively with aqueous 0.5 Ν HCl, saturated aqueous NaHCC , and saturated aqueous NaCl (75 mL each). The organic portion was dried (Na2S04), filtered, and evaporated under reduced pressure. The residue was purified by flash column chromatography (RediSep Gold column, 12 g, gradient elution with 80-100% EtOAc/hexanes) to provide P4-P5-2 (0.28 g, 77%) as a white solid. NMR (500 MHz, CD3OD) δ 7.76 (d, J= 9.0 Hz, 1 H), 7.26 (d, J = 2.5 Hz, 1 H), 7.21 (dd, J= 9.0, 3.0 Hz, 1 H), 5.95 (br s, 1 H), 5.70 (q, J= 8.5 Hz, 1 H), 5.05 (t, J = 9.0 Hz, 1 H), 4.68 (dd, J= 9.0, 7.5 Hz, 1 H), 4.63 (d, J= 11.5 Hz, 1 H), 4.44 (dd, J= 11.5, 3.0 Hz, 1 H), 4.13-4.09 (m, 2 H), 3.94 (s, 3 H), 2.73-2.63 (m, 2 H), 2.57-2.46 (m, 5 H), 2.00-1.93 (m, 1 H), 1.91-1.83 (m, 4 H), 1.72 (dd, J= 8.5, 5.5 Hz, 1 H), 1.64-1.36 (m, 13 H), 1.33-1.26 (m, 1 H), 0.90- 0.84 (m, 2 H), 0.74 (s, 9 H) ppm;13C NMR (125 MHz, CD3OD) δ 179.38, 173.54, 172.91, 171.70, 169.52, 162.05, 156.98, 146.05, 142.68, 136.89, 134.86, 129.27, 126.45, 119.79, 107.34, 76.88, 61.43, 60.87, 56.26, 54.47, 52.16, 45.36, 37.59, 36.09, 35.30, 33.27, 30.92, 28.65, 28.23, 27.87, 27.04, 23.29, 22.37, 21.75, 19.91, 18.43, 14.57, 13.01 ppm; HRMS (ESI) m/z: [M + H]+calcd for C4oH56N709S+, 810.3855; found 810.3836.
77%	With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 5h; Inert atmosphere;	1 (2i?,6A,13aA,14aR,16aA )-6-((A)-2-Acetamido-3,3-dimethylbutanamido)-2-((7-methoxy-3- methylquinoxalin-2-yl)oxy)- V-((l-methylcyclopropyl)sulfonyl)-5,16-dioxo- 1 ,2, 3, 6, 7, 8, 9,10,1 1,13a,l 4,15,16,16a-tetradecahydiOcyclopropa[e] pyrrolo [ 1 ,2- a [ l ,4]diazacyclopentadecine-14a(5//)-carboxamide (P4-P5-2). A mixture of amine salt 11 (0.31 g, 0.45 mmol) and A-Ac-Tle-OH (0.10 g, 0.58 mmol) in anhydrous DMF (8 mL) was treated with DIEA (0.60 mL, 3.50 mmol) and HATU (0.35 g, 0.92 mmol). The resulting reaction mixture was stirred at room temperature for 5 h, then diluted with EtOAc (100 mL), and washed successively with aqueous 0.5 N HC1, saturated aqueous NaHCCT, and saturated aqueous NaCl (75 mL each). The organic portion was dried (NarSOr), filtered, and evaporated under reduced pressure. The residue was purified by flash column chromatography (RediSep Gold column, 12 g, gradient elution with 80-100% EtO Ac/hexanes) to provide P4-P5-2 (0.28 g, 77%) as a white solid. JH NMR (500 MHz, CD3OD) d 7.76 (d, J = 9.0 Hz, 1 H), 7.26 (d, J = 2.5 Hz, 1 H), 7.21 (dd, J= 9.0, 3.0 Hz, 1 H), 5.95 (br s, 1 H), 5.70 (q, J = 8.5 Hz, 1 H), 5.05 (t, J = 9.0 Hz, 1 H), 4.68 (dd, = 9.0, 7.5 Hz, 1 H), 4.63 (d, J= 11.5 Hz, 1 H), 4.44 (dd, = 11.5, 3.0 Hz, 1 H), 4.13-4.09 (m, 2 H), 3.94 (s, 3 H), 2.73-2.63 (m, 2 H), 2.57-2.46 (m, 5 H), 2.00-1.93 (m, 1 H), 1.91-1.83 (m, 4 H), 1.72 (dd, J= 8.5, 5.5 Hz, 1 H), 1.64-1.36 (m, 13 H), 1.33-1.26 (m, 1 H), 0.90- 0.84 (m, 2 H), 0.74 (s, 9 H) ppm; 13C NMR (125 MHz, CD3OD) d 179.38, 173.54, 172.91, 171.70, 169.52, 162.05, 156.98, 146.05, 142.68, 136.89, 134.86, 129.27, 126.45, 119.79, 107.34, 76.88,61.43, 60.87, 56.26, 54.47, 52.16, 45.36, 37.59, 36.09, 35.30, 33.27, 30.92, 28.65, 28.23, 27.87,27.04, 23.29, 22.37, 21.75, 19.91, 18.43, 14.57, 13.01 ppm; HRMS (ESI) m/z: [M + H]+ calcd for C4OH56N709S+, 810.3855; found 810.3836.

Physical hazards
Code	Phrase
H200	Unstable explosive
H201	Explosive; mass explosion hazard
H202	Explosive; severe projection hazard
H203	Explosive; fire, blast or projection hazard
H204	Fire or projection hazard
H205	May mass explode in fire
H220	Extremely flammable gas
H221	Flammable gas
H222	Extremely flammable aerosol
H223	Flammable aerosol
H224	Extremely flammable liquid and vapour
H225	Highly flammable liquid and vapour
H226	Flammable liquid and vapour
H227	Combustible liquid
H228	Flammable solid
H229	Pressurized container: may burst if heated
H230	May react explosively even in the absence of air
H231	May react explosively even in the absence of air at elevated pressure and/or temperature
H240	Heating may cause an explosion
H241	Heating may cause a fire or explosion
H242	Heating may cause a fire
H250	Catches fire spontaneously if exposed to air
H251	Self-heating; may catch fire
H252	Self-heating in large quantities; may catch fire
H260	In contact with water releases flammable gases which may ignite spontaneously
H261	In contact with water releases flammable gas
H270	May cause or intensify fire; oxidizer
H271	May cause fire or explosion; strong oxidizer
H272	May intensify fire; oxidizer
H280	Contains gas under pressure; may explode if heated
H281	Contains refrigerated gas; may cause cryogenic burns or injury
H290	May be corrosive to metals
Health hazards
Code	Phrase
H300	Fatal if swallowed
H301	Toxic if swallowed
H302	Harmful if swallowed
H303	May be harmful if swallowed
H304	May be fatal if swallowed and enters airways
H305	May be harmful if swallowed and enters airways
H310	Fatal in contact with skin
H311	Toxic in contact with skin
H312	Harmful in contact with skin
H313	May be harmful in contact with skin
H314	Causes severe skin burns and eye damage
H315	Causes skin irritation
H316	Causes mild skin irritation
H317	May cause an allergic skin reaction
H318	Causes serious eye damage
H319	Causes serious eye irritation
H320	Causes eye irritation
H330	Fatal if inhaled
H331	Toxic if inhaled
H332	Harmful if inhaled
H333	May be harmful if inhaled
H334	May cause allergy or asthma symptoms or breathing difficulties if inhaled
H335	May cause respiratory irritation
H336	May cause drowsiness or dizziness
H340	May cause genetic defects
H341	Suspected of causing genetic defects
H350	May cause cancer
H351	Suspected of causing cancer
H360	May damage fertility or the unborn child
H361	Suspected of damaging fertility or the unborn child
H361d	Suspected of damaging the unborn child
H362	May cause harm to breast-fed children
H370	Causes damage to organs
H371	May cause damage to organs
H372	Causes damage to organs through prolonged or repeated exposure
H373	May cause damage to organs through prolonged or repeated exposure
Environmental hazards
Code	Phrase
H400	Very toxic to aquatic life
H401	Toxic to aquatic life
H402	Harmful to aquatic life
H410	Very toxic to aquatic life with long-lasting effects
H411	Toxic to aquatic life with long-lasting effects
H412	Harmful to aquatic life with long-lasting effects
H413	May cause long-lasting harmful effects to aquatic life
H420	Harms public health and the environment by destroying ozone in the upper atmosphere

[ CAS No. 22146-59-4 ] {[proInfo.proName]}

Quality Control of [ 22146-59-4 ]

Related Doc. of [ 22146-59-4 ]

Product Details of [ 22146-59-4 ]

Calculated chemistry of [ 22146-59-4 ] Expand+

Physicochemical Properties

Pharmacokinetics

Lipophilicity

Druglikeness

Water Solubility

Medicinal Chemistry

Safety of [ 22146-59-4 ]

Application In Synthesis of [ 22146-59-4 ]

[ 22146-59-4 ] Synthesis Path-Upstream 1~1

[ 22146-59-4 ] Synthesis Path-Downstream 1~19

Technical Information

Related Functional Groups of [ 22146-59-4 ]

Amides

Precautionary Statements-General

Prevention

Response

Storage

Disposal

Physical hazards

Health hazards

Environmental hazards

Inquiry

Related Functional Groups of
[ 22146-59-4 ]