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Chemical Structure| 22179-31-3 Chemical Structure| 22179-31-3

Structure of 22179-31-3

Chemical Structure| 22179-31-3

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Product Details of [ 22179-31-3 ]

CAS No. :22179-31-3
Formula : C10H11ClN2O5S
M.W : 306.72
SMILES Code : O=S(N1CCOCC1)(C2=CC=C(Cl)C([N+]([O-])=O)=C2)=O
MDL No. :MFCD00121800

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Application In Synthesis of [ 22179-31-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 22179-31-3 ]

[ 22179-31-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 110-91-8 ]
  • [ 97-08-5 ]
  • [ 22179-31-3 ]
YieldReaction ConditionsOperation in experiment
24 g With triethylamine; In dichloromethane; at -40℃; for 1h; At -40C, to22g 4-chloro-3-nitrobenzenesulfonyl chloride (CAS97-08-5) in 330ml dichloromethane was added dropwise 18ml of triethylamine and 7.49g morpholine (CAS110-91-8) and stirred at -40C for 1 hour, the temperature was slowly raised to room temperature. Was washed with water and saturated sodium chloride solution, the reaction mixture, with magnesium sulfate and completely concentrated under vacuum. To give 24g of the title compound as a yellow solid.
 

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