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Chemical Structure| 22342-46-7 Chemical Structure| 22342-46-7

Structure of 22342-46-7

Chemical Structure| 22342-46-7

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Product Details of [ 22342-46-7 ]

CAS No. :22342-46-7
Formula : C9H18N2O2S
M.W : 218.32
SMILES Code : O=C(O)CCCC[C@H]1[C@@H](N)[C@@H](N)CS1
MDL No. :MFCD00058173

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Application In Synthesis of [ 22342-46-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 22342-46-7 ]

[ 22342-46-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 121584-52-9 ]
  • [ 22342-46-7 ]
  • C69H121N13O14S [ No CAS ]
YieldReaction ConditionsOperation in experiment
18% 50 mg (0.041 mmol) compound 1 and 11.25 mg cisdiamino biotin in 20 ml MeOH were heated for 1 h underreflux and subsequently, stirred at room temperature overnight. Afier evaporation of the methanol, the remainder wastaken in 10 ml DCM, treated with 9 mg N-bromosuccinim25 ide and then, stirred for 1 hout The acetyl -protected productwas subsequently separated by preparative HPLC and lyophilized. Then, the acetyl-protecting group was removed with 3 ml 0. 1M LiOH in 50% tetrahydrofuran and the finalproduct was isolated by preparative HPLC. Yield: 10 mg(18%).
 

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